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http://dx.doi.org/10.5012/bkcs.2012.33.8.2613

Ni(OH)2 and NiO Nanostructures: Synthesis, Characterization and Electrochemical Performance  

Saghatforoush, Lotf Ali (Department of Chemistry, Payam Noor University)
Hasanzadeh, Mohammad (Drug Applied Research Center, Tabriz University of Medical Sciences)
Sanati, Soheila (Department of Chemistry, Payam Noor University)
Mehdizadeh, Robabeh (Department of Chemistry, Payam Noor University)
Publication Information
Bulletin of the Korean Chemical Society / v.33, no.8, 2012 , pp. 2613-2618 More about this Journal
Abstract
Hydrothermal route have been used in different conditions for preparation of $Ni(OH)_2$ nanostructures. The NiO nanoparticles were obtained by calcining the $Ni(OH)_2$ precursor at $450^{\circ}C$ for 2 h. The effect of sodium dodecyl sulfonate (SDS) as surfactant on the morphology and size of $Ni(OH)_2$ nanoparticles were discussed in detail. X-ray diffraction (XRD), Scanning electron microscopy (SEM), Transmission electron microscopy (TEM) and Fourier transform infrared (FT-IR) spectroscopy were used to characterize the products. The growth mechanism of the as-synthesized nanostructures was also discussed in detail based on the experimental results. Coming up, the NiO nanoparticle modified carbon paste electrode was applied to the determination of captopril in aqueous solution.
Keywords
$Ni(OH)_2$; NiO; Hydrothermal synthesis; Sodium dodecyl sulfonate; Captopril;
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