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http://dx.doi.org/10.5012/bkcs.2012.33.1.123

A Green and Highly Efficient Solvent-free Synthesis of Novel Calicx[4]resorcinarene Derivatives Using Tungstate Sulfuric Acid  

Karami, Bahador (Department of Chemistry, Yasouj University)
Khodabakhshi, Saeed (Department of Chemistry, Yasouj University)
Safikhani, Niloofar (Department of Chemistry, Yasouj University)
Arami, Afsaneh (Department of Chemistry, Yasouj University)
Publication Information
Bulletin of the Korean Chemical Society / v.33, no.1, 2012 , pp. 123-127 More about this Journal
Abstract
A facile and simple procedure for the synthesis of novel and known calix[4]resorcinarene derivatives were developed via a reaction of arylaldehydes with resorcinol in the presence of catalytic amounts of tungstate sulfuric acid (TSA) under solvent-free conditions. This eco-friendly method has many appealing attributes, such as excellent yields, short reactions times, use of safe and recoverable catalyst, and simple work-up procedures. TSA was characterized by powdered X-ray diffraction (XRD), X-ray fluorescence (XRF) and FTIR spectroscopy.
Keywords
Calix[4]resorcinarene; Arylaldehyde; Resorcinol; Tungstate sulfuric acid;
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