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http://dx.doi.org/10.5012/bkcs.2009.30.12.3045

Characterization of Graphene Sheets Formed by the Reaction of Carbon Monoxide with Aluminum Sulfide  

Yoon, Il-Sun (Department of Chemistry, KAIST)
Kim, Chang-Duk (Faculty of Liberal Education, Sangju Campus, Kyungpook National University)
Min, Bong-Ki (Instrumental Analysis Center, Yeungnam University)
Kim, Young-Ki (Center for Research Facilities, Ulsan National Institute of Science and Technology)
Kim, Bong-Soo (Department of Chemistry, KAIST)
Jung, Woo-Sik (School of Display and Chemical Engineering, College of Engineering, Yeungnam University)
Publication Information
Bulletin of the Korean Chemical Society / v.30, no.12, 2009 , pp. 3045-3048 More about this Journal
Abstract
Graphene sheets formed by the reaction of carbon monoxide (CO) with aluminum sulfide ($Al_2S_3$) at reaction temperatures ${\leq}$ 800 $^{\circ}$ were characterized by X-ray diffraction (XRD), Raman spectroscopy, and high-resolution transmission electron microscopy (HRTEM). The graphene sheets, formed as CO was reduced to gaseous carbon by the reaction with $Al_2S_3$, in the temperature range 800 - 1100 $^{circ}C$, did not exhibit their characteristic XRD peaks because of the small number of graphene layers and/or low crystallinity of graphene sheets. Raman spectra of graphene sheets showed that the intensity ratio of the D band to the G band decreased and the 2D band was shifted to higher frequencies with increasing reaction temperature, indicating that the number of graphene layers increased with increasing reaction temperature.
Keywords
Graphene sheets; Carbon monoxide; Aluminum sulfide; Raman spectroscopy;
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