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http://dx.doi.org/10.5012/bkcs.2009.30.10.2265

Polymorphic Forms of Furosemide Characterized by THz Time Domain Spectroscopy  

Ge, Min (Shanghai Institute of Applied Physics, Chinese Academy of Sciences)
Liu, Guifeng (Shanghai Institute of Applied Physics, Chinese Academy of Sciences)
Ma, Shihua (Shanghai Institute of Applied Physics, Chinese Academy of Sciences)
Wang, Wenfeng (Shanghai Institute of Applied Physics, Chinese Academy of Sciences)
Publication Information
Bulletin of the Korean Chemical Society / v.30, no.10, 2009 , pp. 2265-2268 More about this Journal
Abstract
Terahertz time domain spectroscopy (THz-TDS) is applied in transmission to identify the five forms of modifications of furosemide and one commercial product from 0.3 THz to 1.6 THz at room temperature. The different absorption spectra of the different forms are sensitive to crystal structures. Density function theory (DFT) calculation was used to understand the vibrational modes of furosemide in the THz region. X-ray powder diffractometry (XRPD) was applied to confirm the different forms of modifications. The results demonstrate that THz-TDS is a potential analytical technique in investigating polymorphic forms in the pharmaceutical fields.
Keywords
Terahertz; Furosemide; DFT; XRPD; Polymorphic forms;
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1 Haleblian, J. K.; McCrone, W. J. J. Pharm. Sci. 1969, 58, 911.   DOI
2 Trelfall, T. L. Analyst 1995, 120, 2435.   DOI   ScienceOn
3 Brittain, H. G.; Bogdanowich, S. J.; Bugay, D. E.; DeVincentis, J.; Lewen, G.; Newman, A. W. Pharm. Res. 1991, 8, 963.   DOI   ScienceOn
4 Byrn, S.; Pfeiffer, R.; Ganey, M.; Hoiberg, C.; Poochikian, G. Pharm. Res. 1995, 12, 945.   DOI   ScienceOn
5 Yu, L.; Reutzel, S. M.; Stephenson, G. A. Pharmaceut. Sci. Tech. Today 1998, 1, 118.   DOI   ScienceOn
6 Caira, M. R. Top. Curr. Chem. 1998, 198, 163.   DOI
7 Brittain, H. G. J. Pharm. Sci. 1997, 86, 405.   DOI   ScienceOn
8 Tonouchi, M. Nat. Photonics 2007, 1, 97.   DOI   ScienceOn
9 Tadday, P. F.; Bradley, I. V.; Arnone, D. D.; Pepper, M. J. Pharm. Sci. 2003, 92, 831.   DOI   ScienceOn
10 Strachan, C. J.; Rades, T.; Newnham, D. A.; Gordon, K. C.; Pepper, M.; Taday, P. F. Chem. Phys. Lett. 2004, 390, 20.   DOI   ScienceOn
11 Liu, H. B.; Chen, Y.; Zhang, X. C. J. Pharm. Sci. 2007, 92, 927.
12 Matsuda, Y.; Tatsumi, E. Int. J. Pharm. 1990, 60, 11.   DOI   ScienceOn
13 Liu, G. F.; Ma, X. J.; Ma, S. H.; Zhao, H. W.; Ma, M. W.; Ge, M.; Wang, W. F. Chin. J. Chem. 2008, 26, 1257.   DOI   ScienceOn
14 Day, G. M.; Zeitler, J. A.; Jones, W.; Rades, T.; Taday, P. F. J. Phys. Chem. B 2006, 110, 447.   DOI   ScienceOn
15 Fischer, B. M.; Walther, M.; Jepsen, P. U. Phys. Med. Biol. 2003, 47, 3807.   DOI   ScienceOn
16 Shen, Y. C.; Upadhya, P. C.; Linfield, E. H.; Davies, A. G. Appl. Phys. Lett. 2003. 82, 2350.   DOI   ScienceOn
17 Strachan, C. J.; Taday, P. F.; Newnham, D. A.; Gordon, K. C.; Zeitler, J. A.; Pepper, M.; Rades, T. J. Pharm. Sci. 2005, 94, 837.   DOI   ScienceOn
18 Frisch, M. J.; Trucks, G. W.; Schlegel, H. B. et al. Gaussian 03, Revision C.02; Gaussian, Inc.: Wallingford CT, 2004.
19 Doherty, C.; York, P. J. Pharm. Sci. 1987, 76, 731.   DOI
20 Doherty, C.; York, P. Int. J. Pharm. 1988, 47, 141.   DOI   ScienceOn
21 Zeitler, J. A.; Newnham, D. A.; Taday, P. F.; Strachan, C. J.; Pepper, M.; Gordon, K. C.; Rades, T. Thermochimica Acta 2005, 436, 71.   DOI   ScienceOn
22 Fitzgerald, A. J.; Cole, B. E.; Taday, P. F. J. Pharm. Sci. 2004, 94, 177.   DOI   ScienceOn