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http://dx.doi.org/10.5012/bkcs.2006.27.4.524

Preparation of Three Different Style Packed Capillary Frits  

Ryoo, Jae-Jeong (Dept. of Chemistry Education, Kyungpook National University)
Song, Young-Ae (Dept. of Chemistry Education, Kyungpook National University)
Lee, Kwang-Pill (Dept. of Chemistry Education, Kyungpook National University)
Park, Ji-Yeon (Dept. of Chemistry Education, Kyungpook National University)
Choi, Seong-Ho (Dept. of Chemistry, Hannam University)
Hyun, Myung-Ho (Dept. of Chemistry, Pusan National University)
Ohta, Kazutoku (Ceramics Research Institute, National Institute of Advanced Industrial Science and Technology)
Fujimoto, Chuzo (Dept. of Chemistry, Hamamatsu University School of Medicine)
Jin, Ji-Ye (Instrumental Analysis Center, Gifu University)
Takeuchi, Toyohide (Dept. of Chemistry, Gifu University)
Lee, Jung-Whan (K-MAC)
Publication Information
Bulletin of the Korean Chemical Society / v.27, no.4, 2006 , pp. 524-528 More about this Journal
Abstract
Three different style capillary columns, a packed capillary with temporary quartz wool frit, a packed capillary with immobilized frit, and an immobilized packed-capillary, were easily prepared with a commercially available (S)-N-(3,5-dinitro-benzoyl)leucine-N-phenyl-N-alkylamide derived chiral stationary phase. Liquid chromatographic chiral separations of some racemic amino acid derivatives on these columns were performed and the results were compared to each other. The packed capillary with immobilized frit showed some merits in chiral chromatography.
Keywords
Different style frit; Packed-capillary; Immobilized frit; Temporary frit; Chiral chromatography;
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