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http://dx.doi.org/10.5012/bkcs.2004.25.12.1869

Synthesis and Hydrogen-Bonded Supramolecular Assembly of trans-Dihydroxotin(IV) Tetrapyridylporphyrin Complexes  

Jo, Hwa-Jin (Department of Applied Chemistry, Kumoh National Institute of Technology)
Jung, Su-Hee (Department of Applied Chemistry, Kumoh National Institute of Technology)
Kim, Hee-Joon (Department of Applied Chemistry, Kumoh National Institute of Technology)
Publication Information
Bulletin of the Korean Chemical Society / v.25, no.12, 2004 , pp. 1869-1873 More about this Journal
Abstract
trans-Dihydroxo[5,10,15,20-tetrakis(n-pyridyl)porphyrinato]tin(IV) (n = 3 and 4) complexes have been synthesized and fully characterized. X-ray structural analysis of trans-dihydroxo[5,10,15,20-tetrakis(4-pyridyl)porphyrinato]tin(IV) reveals that the supramolecular hydrogen bondings between the hydroxotin(IV) porphyrins and lattice water molecules form a hydrogen-bonded two-dimensional network. The hydrogen bonding mode between the tin(IV) porphyrins and the water molecules closely resembles that of the hydrogenbonded outer-sphere intermediate in the acidolysis of dihydroxotin(IV) porphyrins.
Keywords
Tin(IV); Porphyrins; Hydroxo ligands; Hydrogen bonds; Supramolecular assembly;
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