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http://dx.doi.org/10.5658/WOOD.2019.47.1.1

Phenolic Compounds from Japanese Anise (Illicium anisatum L.) Leaves  

Shinn, Seong-whan (Department of Advanced Materials and Chmemical Engineering, Halla university)
Min, Hee-Jeong (Department of Forest Biomaterials Engineering, College of Forest and Environmental Sciences, Kangwon National University)
Bae, Young-Soo (Department of Forest Biomaterials Engineering, College of Forest and Environmental Sciences, Kangwon National University)
Publication Information
Journal of the Korean Wood Science and Technology / v.47, no.1, 2019 , pp. 1-7 More about this Journal
Abstract
Japanese anise (Illicium anisatum L.) leaves were collected and ground after drying, then immersed with 50 % aqueous acetone for 3 days. After filtration, the extracts were fractionated with n-hexane, chloroform ($CHCl_3$), ethylacetate (EtOAc) and $H_2O$, and then freeze dried after concentration. A portion of EtOAc (3.12 g) and $H_2O$ (6.08 g) soluble fractions were chromatographed on a Sephadex LH-20 column with various aqueous MeOH solution to isolate the compounds. Compound 1 ((+)-catechin) was isolated from EtOAc soluble fraction. Compounds 2 (quercetin), 3 (quercitrin) and 4 (2''-O-rhamnosylvitexin) were isolated from $H_2O$ soluble fraction. For the first time, quercitrin (3) and 2''-O-rhamnosylvitexin (4) of the isolated compounds were obtained from the extracts of japanese anise leaves.
Keywords
Japanese anise (llicium anisatum L); leaves extracts; column chromatography; EtOAc soluble; $H_2O$ soluble;
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