Browse > Article
http://dx.doi.org/10.9713/kcer.2021.59.1.118

Production of Vaterite Type Calcium Carbonate by using Oyster Shell Waste with Lysine  

Bak, Young-Cheol (Department of Chemical Engineering Gyeongsang National University, Engineering Research Institute)
Publication Information
Korean Chemical Engineering Research / v.59, no.1, 2021 , pp. 118-126 More about this Journal
Abstract
The experiments to produce the vaterite type calcium carbonate were conducted for using the waste oyster shell as the recycling resources. Firstly, the oyster shell were calcinated at 800 ℃ for 24 h. Calcinated oyster shell were reacted with the nitric acid solution, and were diluted to 0.1 M Ca(NO3)2 solution. This solution was mixed with 0.1 M Na2CO3 contained 0.1 mol lysine/1 mol CaO at 20 ℃ and 600 rpm mixing condition for 1 h. The reaction products were identified to vaterite type calcium carbonate (84.5% vaterite, 15.5% calcite) by XRD and SEM analysis. Mean particle diameter was 6.87 ㎛, and the lysine content in calcium carbonate was analyzed to 0.1%.
Keywords
Oyster shell; Lysine; Calcium carbonate; Vaterite; $CaCO_3$;
Citations & Related Records
Times Cited By KSCI : 2  (Citation Analysis)
연도 인용수 순위
1 https://www.kmi.re.kr/web/contents View.do?rbsidx=224, Korea Maritime Institute, Marine ocean statics(2018).
2 Park, S. C., Cho, H. S. and Chung, J. D., "Feasibility Study of Paper Filler Recycling using Oyster Shell," Journal of Korea Society of Waste Management, 33(5), 513-520(2016).   DOI
3 Song, S. M., Seong, B. I., Koo, J. H. and Kim, I. H., "Effect of Aspartic Acid and Lysine on Polymorphism of Calcium Carbonate Crystal formed by Gas-liquid Reaction," Korean Chem. Eng. Res., 49(1), 109-113(2011).   DOI
4 Thenepalli, T., Jun, A. Y., Han, C., Ramakrishna, C., Ahn, J. W., "A Strategy of Precipitated Calcium Carbonate (CaCO3) Fillers for Enhancing the Mechanical Properties of Polypropylene Polymers," Korean J. Chem. Eng., 32(6), 1009-1022(2015).   DOI
5 Maruo Calcium, "Monodispersed Vaterite type Calcium Carbonate, and Shape Control Method," Korea Patent No 10-0176250(1998).
6 KAIST, "Method for preparing Hydroxyapatite from Vaterite containing Catechol Amine," Korea Patent No 10-1318348(2013).
7 Lyu, S. G,, Ryu, S. O., Park, Y, H. and Sur, G. S., "The preparation of Spherical Vaterite in the presence of NH4Cl by Carbonation Process," Korean Chem. Eng. Res., 36(2), 262-266(1998).
8 Kang, Y. C. and Park, S. B., "Preparation of Cubic-type Calcium Carbonate particles from High Concentration Calcium Hydroxide Suspension by Controlling Hydration Temperature of Calcium Oxide," Korean Chem. Eng. Res., 35(6), 846-849(1997).
9 Lee, S. G., Jung, W. M., Kim, W. S. and Choi, C. K., "Effect of Agitation on Gas-Liquid Reaction Crystallization of Calcium Carbonate in an MSMPR Reactor," Korean Chem. Eng. Res., 36(1), 49-55(1998).
10 Saksono, N., Gozan, M., Bismo, S, Krisanti, E., Widaningrum, R. and Song, S. K., "Effects of Magnetic Field on Calcium Carbon ate Precipitation : Ionic and Particle Mechanism," Korean J. Chem. Eng., 25(5), 1145-1150(2008).   DOI
11 Han, H. K., Kim, B. M. and Kim, J. A., "Influence of Temperatures and PAA Solution in the Formation of Calcium Carbonate Crystal," Korean Chem. Eng. Res., 46(6), 1052-1056(2008).
12 Kim, J. H., Kim, J. M., Kim, W. S. and Kim, I. H., "Polymorphism of Calcium Carbonate Crystal by Silk Digested Amino Acid," Korean Chem. Eng. Res., 46(6), 1107-1112(2008).
13 Song, S. M., Seong, B. I., Koo, J. H. and Kim, I. H., "Effect of Aspartic Acid and Lysine on Polymorphism of Calcium Carbonate Crystal Formed by Gas-Liquid Reaction," Korean Chem. Eng. Res., 49(1), 109-113(2011).   DOI
14 Kim, J. H., Kim, J. M., Kim, W. S. and Kim, I. H., "Polymorphism of Calcium Carbonate Crystal by addition of various Amino," Korean Chem. Eng. Res., 47(2), 213-219(2009).
15 Kim, J. H., Song, S. M., Kim, J. M., Kim, W. S. and Kim, I. H., "CaCO3 Crystallization with feeding of Aspartic Acid," Korean J. Chem. Eng., 27(5), 1532-1537(2010).   DOI
16 Son, C., Song, W., Hwang D. S., Hong, Y. K., Joo, J. and Choi, Y. S., "Recombinant Production and Biochemical Characterization of a Hypothetical Acidic Shell Matrix Protein in Escherichia Coli for the preparation of Protein-based CaCO3 Biominerals," Korean J. Chem. Eng., 33(8), 2406-2410(2016).   DOI
17 Kralj, D. and Brecevic, L., "Vaterite Growth and Dissolution in Aqueous Solution 1. Kinetics of Crystal growth," J. Crystal Growth, 104, 793-800(1990).   DOI
18 Ogino, T., Suzuki, T. and Sawada, K., "The Rate and Mechanism of Polymorphic Transfomation of Calcium Carbonate in Water," Journal of Crystal Growth, 100, 159-167(1990).   DOI
19 Albeck, S., Weiner, S. and Addadi, L., "Polysaccharides of Intracrystalline Glycoproteins Modulate Calcite Crystal Growth In vitro," Chem. Eur. J., 2(3), 278-284(1996).   DOI
20 Zhang, S. and Gonsalves, K. E., "Influence of the Chitosan Surface Profile on the Nucleation and Growth of Calcium Carbonate Films," Langmuir, 14, 6761-6766(1998).   DOI
21 Rao, M. S., "Kinetics and Mechanism of the Transformation of Vaterite to Cacite," Bulletin of the Chemical Society of Japan, 46, 1414-1417(1973).   DOI
22 Kontoyannis, C. and Vagenas, N. V., "Calcium Carbonate Phase Analysis using XRD and FT-Raman Spectroscopy," Analyst, 125, 251-255(2000).   DOI
23 Han, H. K., Jeong, O. H., Lim, M. H. and Kim, J. A., "Effect of RPM and Temperature on the CSD in the CMSMPR Calcium Carborate Crystallization," Korean Chem. Eng. Res., 44(3), 289-293(2006).
24 Lyu, S. G., Sur, G. S. and Kang, S. H., "A Study of Crystal Shape of the precipitated Calcium Carbonate formed in the Emulsion State," Korean Chem. Eng. Res., 35(2), 186-191(1997).