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Quartz Crystal Microbalance Modified by a Novel Vapor Diffused Molecular Assembly Technique and Measurement of Chiral Mandelic Acid  

Kim, JongMin (Department of Chemical Engineering, Dong-A University)
Kim, SeungJin (Department of Chemical Engineering, Dong-A University)
Woo, SunYoung (Department of Chemical Engineering, Dong-A University)
Jang, SukHee (Department of Chemical Engineering, Dong-A University)
Kim, Woo-Sik (Department of Chemical Engineering)
Chang, SangMok (Department of Chemical Engineering, Dong-A University)
Publication Information
Korean Chemical Engineering Research / v.48, no.5, 2010 , pp. 574-582 More about this Journal
Abstract
In this study, the possibility of a quartz crystal micro-balance(QCM) modification of crystallization of L-Penicillamine and D-Penicillamine with a Vapor Diffused Molecular Assembly Technique and its application to the R-(-)-Mandelic acid and S-(+)- Mandelic acid measurement was investigated. The 3-dimensional structures of L-Penicillamine and D-Penicillamine on the surface of QCM were verified to be different from each other through QCM and AFM analyses. The D-Penicillamine modified QCM had specific recognition to the R-(-)-Mandelic acid, but L-Penicillamine modified QCM had no specificity to the R-(-)-Mandelic acid and S-(+)- Mandelic acid. From these results, it was known that the QCM could be modified with various selective meterials via VDMA, and the chiral isomer such as a Mandelic acid isomer could be detected by using a modified QCM.
Keywords
Chiral Recognition; Quartz Crystal Microbalance; Mandelic Acid; Vapor Diffused Molecular Assembly; Penicillamine; Receptor;
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