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Determination of Unimark 1494DB in Petroleum using HPLC  

Lim, Young-Kwan (Research Center, Korea Institute of Petroleum Management)
Kim, DongKil (Research Center, Korea Institute of Petroleum Management)
Yim, Eui Soon (Research Center, Korea Institute of Petroleum Management)
Shin, Seong-Cheol (Research Center, Korea Institute of Petroleum Management)
Publication Information
Korean Chemical Engineering Research / v.47, no.5, 2009 , pp. 593-598 More about this Journal
Abstract
In this study, the qualitative and quantitative analytical method for petroleum marker(Unimark 1494DB) in common diesel involved kerosene and byproduct fuel was developed using SPE pretreatment and high performance liquid chromatography. In SPE pretreatment process, the highest concentrated marker was obtained 15 minutes after addition of petroleum sample. The petroleum marker was detected with $1626.92mV{\cdot}sec$ intensity at 9.8 minutes retention time in 1 mg/L content in petrodiesel after pretreatment. Also petroleum marker was selectively identified in an acidic petroleum product which was previously difficult to be analyzed by UV-Vis Spectroscopy.
Keywords
Petroleum Marker; Unimark 1494DB; SPE(Solid phase extraction); HPLC; ELSD;
Citations & Related Records
Times Cited By KSCI : 5  (Citation Analysis)
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