Determination of Captan, Folpet, Captafol and Chlorothalonil Residues in Agricultural Commodities using GC-ECD/MS
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Lee, Su-Jin
(Dept. of Herbal Medicine Resource, Kangwon National University)
Hwang, Young-Sun (Dept. of Herbal Medicine Resource, Kangwon National University) Kim, Young-Hak (Dept. of Herbal Medicine Resource, Kangwon National University) Kwon, Chan-Hyeok (Food Chemical Residues Division, NIFDS, KFDA) Do, Jung-A (Food Chemical Residues Division, NIFDS, KFDA) Im, Moo-Hyeog (Food Standardization Division, KFDA) Lee, Young-Deuk (Division of Life and Environmental Science, Daegu University) Choung, Myoung-Gun (Dept. of Herbal Medicine Resource, Kangwon National University) |
1 | Zhao, L., Fan, D.F., 1996. Gas chromatographic determination of chlorothalonil in leaves and roots of scrophularia and in soil, J. Assoc. Off. Anal. Chem. 79, 587-588. |
2 | Zweig, G., Sherma, J., 1978. Analytical methods for pesticides and plant growth regulators, Vol. VI, pp. 546-549 and 556-560, Academic Press, NY, USA. |
3 | Lee, J., Park, H., Keum, Y., Kwon, C., Lee, Y., Kim, J., 2008. Dissipation pattern of boscalid in cucumber under green house condition, Kor. J. Pestic. Sci. 12, 67-73. |
4 | Lee, Y.D., 2009. Manual of official method of analysis for pesticide residues in foods, Korea food and drug adiministration. |
5 | Martinez, R.C., Gonzalo, E.R., Jimenez, M.G.G., Pinto, C.G., Pavon, J.L.P., Mendez, J.H., 1996. Determination of the fungicides folpet, captan and captafol by cloud-point preconcentration and high-performance lquid chromatography with electrochemical detection, J. Chromatogr. A 754, 85-96. DOI ScienceOn |
6 | Miller, J.M., 2005. Chromatography: Concepts and Contrasts, 2nd ed., pp. 286-287, Wiley Intersciense, USA. |
7 | Neger, B.O., Foster, G.D., Khan, S.U., 2000. Determination of chlorothalonil residues in coffee, Toxicotogical and Environmental Chemistry, 77, 41-47. DOI ScienceOn |
8 | Park, C.J., Lee, Y.D., 2003. Persistence of the fungicide boscalid in grapes and strawberries, Life Sci. Res. 2(2), 9-16. |
9 | Penuela, G.A., Barceló, D., 1998. Photodegradation and stability of chlorothalonil in water studied by solid-phase disk extraction, followed by gas chromatographic techniques, Chromatographia A 823, 81-90. |
10 | Pomerantz, I.H., Ross, R., 1968. Captan and structurally related compounds, thin-layer and gas liquid chromatography, J. Assoc. Off. Anal. Chem. 51, 1058-1062. |
11 | US FDA, 1999. Pesticide Analytical Manual, Vol 1: Multi-residue Methods, 3rd ed., US Food and Drug Administration, USA. |
12 | Korea Food and Drug Administration, 2009. Maximum residue limits for pesticides in foods. |
13 | Kwon, C.H., Lee, Y.D., 2003. Terminal residues of monocrotophos and phosphamidon in apples, Life Sci. Res. 1(3), 277-286. |
14 | Akiyama, Y., Yano, M., Mitsuhashi, T., Takeda, N., Tauji, M., 1996. Simultaneous determination of pesticides in agricultural products by solid-phase extraction and gas chromatography-mass spectrometry, J. Food Hyg. Soc. 37, 351-362. DOI ScienceOn |
15 | AOAC, 2000. Pesticide and industrial chemical residues, In official method of analysis, 17th ed., pp. 1-88, AOAC International, Arlington, VA, USA. |
16 | Carlstrom, A.A., 1971. Collaborative study of a gas chromatographic method for determining captan in formulations, J. Assoc. Off. Anal. Chem. 54, 688-696. |
17 | Codex Alimentarius Commission, 2003. Guidelines on good laboratory practice in residue analysis, CAC/ GL 40-1993, Rev.1-2003, Rome, Italy. |
18 | Daroon, C.V., Vink, M., Poll, J.M.V.D., 1995. Gas chromatographic determination of chlorothalonil and its metabolite 4-hydroxy-2,5,6-trichloro-isophtalonitrile (HTI) in water, Chromatographia 40, 458-462. DOI |
19 | Fillion, J., Sauve, F., Selwyn, J., 2000. Multi residue method for the determination of residues of 251 pesticides in fruits and vegetables by gas chromatography/ mass spectrometry and liquid chromatography with fluorescence detection, J. Assoc. Off. Anal. Chem. 83, 698-713. |
20 | Fishbein, L., 1973. Chromatography of environmental hazards, Vol. I, pp.169-179, Elsevier, NY, USA. |
21 | Fong, W.G., Moye, H.A., Seiber, J.N., Toth, J.P., 1999. Pesticide Residues in Food: Methods, Technologies, and Regulations, pp. 3-4 and 40-44, Wiley Interscience, Canada. |
22 | Francoeur, Y., Mallet, V., 1977. Simultaneous determination of captan and captafol in apples and potatoes by thin layer chromatography and in situ fluorometry, J. Assoc. Off. Anal. Chem. 60, 1328-1330. |
23 | Jung, Y.H., Kim, J.E., Kim, J.H., Lee, Y.D., Im, C.H., Hur, J.H., 2004. Pesticide Science, 2nd ed., Sigma Press, Seoul, Korea, pp.197. |
24 | Korea Food and Drug Administration, 2009. Korean code of food. |
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