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http://dx.doi.org/10.14579/MEMBRANE_JOURNAL.2016.26.4.318

Preparation and Characterization of Polysaccharide-based Nanofiber Using Electrospinning Method  

Kim, Se Jong (Department of Materials Engineering and Convergence Technology, Gyeongsang National University)
Lee, Su Jeong (Department of Materials Engineering and Convergence Technology, Gyeongsang National University)
Woo, Chang Hwa (Director of Planning Center, Gyeongsang National University Academy and Industry Collaboration)
Nam, Sang Yong (Department of Materials Engineering and Convergence Technology, Gyeongsang National University)
Publication Information
Membrane Journal / v.26, no.4, 2016 , pp. 318-327 More about this Journal
Abstract
In this study, alginate/poly(ethylene oxide) (PEO), and chitosan/PEO solution are prepared by dissolving alginate and chitosan into specific solvent for electrospinning. Solutions are poured into 10 mL plastic syringes with a metal nozzle supplied a high voltage power. The solution of alginate and chitosan is controlled by polymer concentration, temperature, relative humidity, applied voltage, distance from nozzle and flow rate of solution. Morphologies of fabricated nanofiber are observed by scanning electron microscopy (SEM). Optimal conditions for electrospinning of alginate nanofiber membrane are 2 wt% of alginate, 2 wt% of PEO at $60^{\circ}C$, 15 cm from the nozzle, $8{\mu}m/min$ flow rate and 20~24 kV. The conditions for elctrospinning of chitosan nanofiber membrane are 2 wt% of chitosan, 2 wt% PEO at $25^{\circ}C$, 15 cm from the nozzle, $8{\mu}m/min$ flow rate and 24 kV. The fabrication conditions of complex nanofiber prepared with chitosan and alginate are 20 cm from the nozzle, $8{\mu}m/min$ flow rate and 26 kV.
Keywords
electrospinning; nanofiber; alginate; chitosan; poly(ethylene oxide);
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