We report the phase transition temperatures of the perovskite nanotubes made by sol-gel template synthesis. The lead zirconate() nanotubes were prepared with a chelate sol-gel of zirconium tetrabutoxide() and leadacetate(). anodisc membranes, with a 200nm pore size, served as the template. After removing the template in the 6M-NaOH solution, the nanotubes so far have shown an anomalous transition temperature, as measured by DSC with a small particle size, 15.4nm determined by X-ray analysis with the aid of Scherrer's equation.
Keywords
sol-gel template synthesis; lead zirconate() nanotubes;