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http://dx.doi.org/10.5850/JKSCT.2010.34.6.1042

GC-MS Analysis of Amur Cork Tree Extract and Its Degradation Products  

Ahn, Cheun-Soon (Dept. of Fashion Industry, University of Incheon)
Publication Information
Journal of the Korean Society of Clothing and Textiles / v.34, no.6, 2010 , pp. 1042-1052 More about this Journal
Abstract
The Degradation of amur cork tree extract is investigated by GC-MS after treating the dye with three thermal degradation systems of, room temperature (RT), $4^{\circ}C$ refrigeration (LT), $100^{\circ}C$ oven (OV), and $H_2O_2$/UV/$O_2$ (PER) degradation system for 0-24 days. It was found that PER degradation system represented the highest intensity of degradation treatment followed by OV treatment among the four degradation parameters. The possible fingerprint products of amur cork tree dye, that yielded 68% (or higher) reliability in the NIST spectral match, were isobenzofuran-1,3-dione,4,5-dimethoxy- (8.37 min, PER only), 1,3-dioxolo[4,5-g]isoquinolin-5(6H)-one,7,8-dihydro (9.41 min, PER only), canthine-6-one (10.24 min, RT, LT, OV only), and dihydroberberine (15.05 min, RT, LT, OV, PER) in the order of higher to lower possibility of detection. Unknown products 7 (13.43 min) and 8 (16.35 min) are two other possible fingerprint products of amur cork tree dye that require future identification.
Keywords
Amur cork tree; Berberine; Degradation; GC-MS; Dye identification;
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Times Cited By KSCI : 4  (Citation Analysis)
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