Browse > Article
http://dx.doi.org/10.6111/JKCGCT.2012.22.6.286

Synthesis of boehmite powder from aluminum etching solution  

Park, Young-Soo (Icheon Branch, Korea Institute of Ceramic Engineering and Technology)
Wui, In-Hee (Icheon Branch, Korea Institute of Ceramic Engineering and Technology)
Cho, Woo-Seok (Icheon Branch, Korea Institute of Ceramic Engineering and Technology)
Kim, Jin-Ho (Icheon Branch, Korea Institute of Ceramic Engineering and Technology)
Hwang, Kwang-Taek (Icheon Branch, Korea Institute of Ceramic Engineering and Technology)
Publication Information
Journal of the Korean Crystal Growth and Crystal Technology / v.22, no.6, 2012 , pp. 286-290 More about this Journal
Abstract
Boehmite (AlOOH) powder was synthesized using waste aluminium etching solution. In waste solution, precipitated phase was gibbsite ($Al(OH)_3$), and boehmite (AlOOH) phase was obtained at pH of 7 and 8 controlled by addition of acid. Boehmite powder was obtained by washing process to remove the Na ion in precipitated solution. Mean particle size of obtained powder was 40 nm. Boehmite phase transformed to ${\alpha}-Al_2O_3$ phase via ${\gamma}-Al_2O_3$, ${\delta}-Al_2O_3$, and ${\Theta}-Al_2O_3$.
Keywords
Aluminum etching; Boehmite; Alumina; Precipitation;
Citations & Related Records
Times Cited By KSCI : 2  (Citation Analysis)
연도 인용수 순위
1 F. Habashi, "Bayer's process for alumina production : A historical perspective", Bull. Hist. Chem 17/18 (1995) 15.
2 A. Al Sadi, E. Bonetti, P. Mattioli and G. Valdre, "Internal friction, thermal and structural analysis of nanocrystalline aluminium", J. Alloys Compounds 211-1 (1994) 489.   DOI   ScienceOn
3 E. Bonetti, G. Scipione, G. Valdre, S. Enzo, R. Frattini and P.P. Macri, "A study of nanocrystalline iron and aluminum metals and fe-al intermetallic by mechanical alloying", J. Mater. Sci. 30 (1995) 2220.   DOI
4 Dariusz Oleszak and Paul H. Shingu, "Nanocrystalline metals prepared by low energy ball milling", J. Appl. Phys. 79 (1996) 2975.   DOI
5 H.H. Jo, S.K. Lee, C.S. Jung and B.M. Kim, "A nonsteady state fe analysis of al tubes hot extrusion by porthole die", J. Mat. Process Tech. 173 (2006) 223.
6 S.G. Woo and H.R. Lee, "Tungsten wire tip sharpening by electrochemicl etching", J. Kor. Institute of Information Sci. and Eng. 31 (1998) 45.
7 K. Wefers and C. Misra, "Oxides and Hydroxides of Aluminum", ALCOA Laboratories, Pennsylvania, USA (1987) p. 20.
8 G. Paglia, C.E. Buckley, A.L. Rohl, R.D. Hart, K. Winter, A.J. Studer, B.A. Hunter and J.V. Hanna, "Boehmite derived $\gamma$-alumina system. 1. Structural evolution with temperature, with the identification and structural determination of a new transition phase, $\gamma$-alumina", Chem. Mater. 16 (2004) 220.   DOI   ScienceOn
9 X. Krokidis, P. Raybaud, A.E. Gobichon, B. Rebours, P. Euzen and H. Toulhoat, "Theoretical study of the dehydration process of boehmite to $\gamma$-alumina", J. Phys. Chem. B 105 (2001) 5121.   DOI   ScienceOn
10 S.J. Wilson, "The dehydration of boehmite, AlOOH, to $Al_{2}O_{3}$", J. Solid State Chem. 30 (1979) 247.   DOI   ScienceOn
11 H.C. Stumpf, A.S. Russell, J.W. Newsome and C.M. Tucker, "Thermal transformations of aluminas and alumina hydrates", Ind. Eng. Chem. 42 (1950) 1398.   DOI
12 H. Cho and B.W. Lee, "High temperature properties of surface-modified Hastelloy X alloy", Journal of the Korean Crystal Growth and Crystal Technology 22/4 (2012) 183.   DOI   ScienceOn
13 H.J. Jeong, J.H. Lee and S.J. Boo, "Investigation of aluminium- induced crystallization of amorphous silicon and crystal properties of the silicon film for polycrystalline silicon solar cell fabrication", Journal of the Korean Crystal Growth and Crystal Technology 20/6 (2010) 254.   과학기술학회마을   DOI   ScienceOn
14 B.C. Lippens and J.H. de Boer, "Study of phase transformations during calcination of aluminum hydroxides by selected area electron diffraction", Acta Crystallogr. 17 (1964) 1312.   DOI
15 G.W. Brindley and I.R. Haya, "Crystallographic aspects of some decomposition and recrystallization reactions", Progress in Ceramic Science Oxford Pergamon Press 3 (1963) p. 3.
16 R.K. Oberlander, "Aluminas for catalysts: their preparation and properties", Applied Industrial Catalysis 3 Chapter 4, Academic Press (1984) p. 63.