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http://dx.doi.org/10.6111/JKCGCT.2010.20.6.295

Solid-state metathetic synthesis of MWO4 (M=Zn, Co) particles assisted by microwave irradiation  

Lim, Chang-Sung (Department of Advanced Materials Science & Engineering, Hanseo University)
Publication Information
Journal of the Korean Crystal Growth and Crystal Technology / v.20, no.6, 2010 , pp. 295-300 More about this Journal
Abstract
Metathetic route for the $MWO_4$ (M=Zn, Co) particles is a simple method of synthesis and a viable alternative method in a short time. $MWO_4$ (M=Zn, Co) particles were synthesized using solid-state metathetic (SSM) method with microwave irradiation. The $MWO_4$ (M=Zn, Co) particles were formed completely at $600^{\circ}C$ for 3 h. The crystallization process, thermal decomposition and morphology of the $MWO_4$(M= Zn, Co) particles were evaluated. The characteristics of the SSM reaction and the formation of a high lattice energy by-product NaCl were discussed.
Keywords
Solid-state metathetic (SSM) synthesis; $ZnWO_4$; $CoWO_4$; Microwave irradiation;
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