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http://dx.doi.org/10.3740/MRSK.2006.16.10.599

Preparation of Silica Core-Hybrid Pigment via Sol-Gel Process and It's Application for Inkjet Dispersion Ink  

Jeon, Young-Min (Department of Chemistry and Institute of Basic Science, Dankook University)
Kim, Jong-Gyu (Department of Chemistry and Institute of Basic Science, Dankook University)
Gong, Myoung-Seon (Department of Chemistry and Institute of Basic Science, Dankook University)
Publication Information
Korean Journal of Materials Research / v.16, no.10, 2006 , pp. 599-605 More about this Journal
Abstract
N-(3-triethoxysilylpropyl)-1,4-diaminoanthrquinone-2,3-dicarboximide (TESP-DADI), an organic blue pigment, has been prepared and incorporated into silica solid matrix reacting triethyl orthosilicate (TEOS) via sol-gel method. Morphology and microstructure of resulting hybrid pigment were studied employing SEM and TEM. The micrographs and particle size distributions showed that uniform pigment can be obtained employing TEOS-based sol-gel method forming silica core. Particle size distribution of dispersed pigment in water was examined using the technique of dynamic light scattering. The ensuing pigment dispersion ink was subjected to various physicochemical evaluation such as viscosity, surface tension, inkjet stability, storage stability, and color change as inkjet ink using spectrophotometric, and microscopic techniques.
Keywords
Blue Anthraquinone dye; sol-gel process; hybrid pigment; inkjet dispersion ink;
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