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http://dx.doi.org/10.3740/MRSK.2002.12.6.458

Characteristics of Carbon Nanotube with Synthetic Conditions in Catalytic Chemical Vapor Deposition  

Kim, Hyeon-Jin (단국대학교, 신소재공학과)
Lee, Im-Ryeol (단국대학교, 신소재공학과)
Publication Information
Korean Journal of Materials Research / v.12, no.6, 2002 , pp. 458-463 More about this Journal
Abstract
Carbon nanotubes were synthesized at various conditions using Ni-catalytic thermal chemical vapor deposition method and their characteristic properties were investigated by SEM, TEM and Raman spectroscopy. Carbon nanotubes were formed on very fine Ni-catalytic particles. The carbon nanotubes synthesized by thermal decomposition of acetylene at $700^{\circ}C$ had a coiled shape, while those synthesized at $850^{\circ}C$ showed a curved and Y-shape having a bamboo-like morphology. It was found that the carbon nanotube was also made on the fine Ni-catalytic particles formed on the surface of 100~400nm sized large ones after pretreatment with $NH_3$.ber composites show the high dielectric constant and large conduction loss which is increased with anisotropy of fiber arrangement. It is, therefore, proposed that the glass and carbon fiber composites can be used as the impedance transformer (surface layer) and microwave reflector, respectively. By inserting the foam core or honeycomb core (which can be treated as an air layer) between glass and carbon fiber composites, microwave absorption above 10 dB (90% absorbance) in 4-12 GHz can be obtained. The proposed fiber composites laminates with sandwitch structure have high potential as lightweight and high strength microwave absorbers.
Keywords
catalytic CVD; carbon nanotube; morphology;
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