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http://dx.doi.org/10.7853/kjvs.2020.43.3.189

Feasibility of monitoring of fluoroquinolones residual through feather analysis in broilers  

Kim, Jae-Ho (Gyeonggi Province Northern Animal Hygiene Laboratory Office)
Kim, Mi-Hee (Gyeonggi Province Northern Animal Hygiene Laboratory Office)
Ahn, Gil-Ho (Gyeonggi Province Northern Animal Hygiene Laboratory Office)
Publication Information
Korean Journal of Veterinary Service / v.43, no.3, 2020 , pp. 189-196 More about this Journal
Abstract
This study was conducted to analyze feasibility of monitoring of fluoroquinolnes residual through feather analysis in broilers. The calibration curve showed good linearity (r2≥0.99) within the concentration range of 1~100 ㎍/kg. The limit of detection (LOD) and limit of quantification (LOQ) were validated at ≤0.66 and ≤1.99 ㎍/kg in broiler feather, respectively. The recoveries in feather samples ranged from 94.6 to 114.4% (5.1-15.8% RSD) at the 5 to 20 ㎍/kg spiking levels. The proposed new analytical method proved to be suitable and effective for fluoroquinolnes determination. We also monitored fluoroquinolones residue in 36 samples (broiler that were slaughtered in Gyonggi-do) using this method. Among tested feather samples, enrofloxacin and ciprofloxacin were detected in all samples. In muscle samples, enrofloxacin was detected in 20 (55.6%) samples and ciprofloxacin was not detected.
Keywords
Fluoroquinolnes; Enrofloxacin; Feather; Monitoring; LC-MS/MS;
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Times Cited By KSCI : 2  (Citation Analysis)
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