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http://dx.doi.org/10.7853/kjvs.2015.38.4.259

Monitoring for cephalosporins residues in raw meat in Seoul  

Kim, Mi-Ran (Seoul Metropolitan Government Research Institute of Public Health ＆ Environment)
Choi, Yoon-Hwa (Seoul Metropolitan Government Research Institute of Public Health ＆ Environment)
Choi, Hoon (Seoul Metropolitan Government Research Institute of Public Health ＆ Environment)
Kim, Doo-Hwan (Seoul Metropolitan Government Research Institute of Public Health ＆ Environment)
Kim, Young-Seob (Seoul Metropolitan Government Research Institute of Public Health ＆ Environment)
Lee, Ju-Hyung (Seoul Metropolitan Government Research Institute of Public Health ＆ Environment)
Publication Information
Korean Journal of Veterinary Service / v.38, no.4, 2015 , pp. 259-264 More about this Journal
Abstract
We investigated the residues of 6 cephalosporins (cefquinome, cephalexin, cephalonium, cefazolin, ceftiofur, cefuroxime) using LC-MS/MS in raw meat in Seoul. This method involves extraction of the residue from the meat by distilled water and methanol followed by a manual of residue analysis published by the National Institute of Food and Drug Safety Evaluation. The recoveries ranged between 74.71~90.01% in beef, 73.37~101.40% in pork and 70.87~95.53% in chicken, respectively. The limits of detection were 0.0004~0.0563 mg/kg, and the limits of quantification were 0.001~0.169 mg/kg respectively. Residues of cephalosporins which exceeded maximum residue limits (MRL) were not exceed in any of the 287 samples. However, it is necessary to develop multi-method, which includes the active metabolites of ceftiofur.
Keywords
Cephalosporins residues; Raw meat; LC-MS/MS;
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