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Simultaneous Determination of Sulfonamides in Porcine and Chicken Muscle Using High Performance Liquid Chromatography with Ultraviolet Detector  

Shim, You-Sin (Korea Food Research Institute)
Shin, Dong-Bin (Korea Food Research Institute)
Cho, Yong-Sun (Korea Food Research Institute)
Choi, Yun-Hee (Korea Food Research Institute)
Lee, Sang-Hee (Korea Food Research Institute)
Publication Information
Food Science and Biotechnology / v.18, no.6, 2009 , pp. 1430-1434 More about this Journal
Abstract
The present study used the liquid extraction pretreatment method and developed a liquid chromatographyultraviolet detector (LC-UV) for the simultaneous determination of 14 sulfonamides (SAs) residues in porcine and chicken muscle. Linearity within a range of $50-150\;{\mu}g/kg$ was obtained with the correlation coefficient ($r^2$) of 0.9673-0.9997. The mean recovery of SAs was 55.9-109.7% (relative standard deviations; RSDs 1.7-17.3%) in porcine muscle and 52.8-112.4% (RSDs 2.3-16.9%) in chicken muscle. The limits of detection (LODs) and limits of quantification (LOQs) were 2-32 and $7-96\;{\mu}g/kg$ in porcine muscle, and 4-32 and $13-97\;{\mu}g/kg$ in chicken muscle, respectively. These values were lower than the maximum residue limits (MRLs) established by the European Union. The sum of all SAs residues present should be less than $100\;{\mu}g/kg$.
Keywords
sulfonamide; porcine muscle; chicken muscle; liquid-liquid extraction (LLE); high performance liquid chromatography-ultraviolet detector (HPLC-UVD);
Citations & Related Records
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Times Cited By Web Of Science : 0  (Related Records In Web of Science)
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