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http://dx.doi.org/10.5478/MSL.2011.2.2.045

Effective Analysis of Dicyclanil in Lamb and Chicken Muscle using HPLCUV/Vis and LC/MS/MS  

Kim, Byung-Ju (Department of Chemistry, Kyonggi University)
Myung, Seung-Woon (Department of Chemistry, Kyonggi University)
Publication Information
Mass Spectrometry Letters / v.2, no.2, 2011 , pp. 45-48 More about this Journal
Abstract
The authors describe a method for monitoring dicyclanil levels in lamb and chicken muscle tissues. The devised procedure involves dicyclanyl extraction by SPE and its detection HPLC-UV/Vis and LC/MS/MS. The method was found to have LOD and LOQ values of $0.02\;mg\;kg^{-1}$ and $0.05\sim0.06\;mg\;kg^{-1}$, respectively. The intraday precision and an accuracy of spiked samples were found to have 2.3~10.4 RSD% and 80.9~105.7%, respectively.
Keywords
Dicyclanil; Lamb; Chicken; Veterinary Drugs; HPLC; LC/MS/MS;
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