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http://dx.doi.org/10.1016/j.jiec.2018.08.016

Implementation of magnetic Fe3O4@ZIF-8 nanocomposite to activate sodium percarbonate for highly effective degradation of organic compound in aqueous solution  

Sajjadi, Saeed (Research Laboratory of Advanced Water and Wastewater Treatment Processes, Department of Applied Chemistry, Faculty of Chemistry, University of Tabriz)
Khataee, Alireza (Research Laboratory of Advanced Water and Wastewater Treatment Processes, Department of Applied Chemistry, Faculty of Chemistry, University of Tabriz)
Soltani, Reza Darvishi Cheshmeh (Department of Environmental Health Engineering, School of Health, Arak University of Medical Sciences)
Bagheri, Nafiseh (Research Laboratory of Advanced Water and Wastewater Treatment Processes, Department of Applied Chemistry, Faculty of Chemistry, University of Tabriz)
Karimi, Afzal (Faculty of Advanced Technologies in Medicine, Iran University of Medical Sciences)
Azar, Amirali Ebadi Fard (Faculty of Medicine, Iran University of Medical Sciences)
Publication Information
Journal of Industrial and Engineering Chemistry / v.68, no., 2018 , pp. 406-415 More about this Journal
Abstract
Here, as-synthesized $Fe_3O_4$ nanoparticles were incorporated into the zeolitic imidazolate framework (ZIF-8) lattice to activate sodium percarbonate (SPC) for degradation of methylene blue (MB). The reaction rate constant of $Fe_3O_4@ZIF-8/SPC$ process ($0.0632min^{-1}$) at acidic conditions (pH = 3) was more than six times that of the $Fe_3O_4/SPC$ system ($0.009min^{-1}$). Decreasing the solute concentration, along with increasing SPC concentration and $Fe_3O_4@ZIF-8$ nanocomposite (NC) dosage, favored the catalytic degradation of MB. The $Fe_3O_4@ZIF-8$ NC after fifteen consecutive treatment processes showed the excellent stability with a negligible drop in the efficiency of the system (<10%). The reaction pathway was obtained via GC-MS analysis.
Keywords
Chemical oxidation; Zeolitic imidazolate framework; Magnetite nanostructures; Textile dye; Solid hydrogen peroxide;
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