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http://dx.doi.org/10.1016/j.jiec.2018.06.036

Distillation design and optimization of quaternary azeotropic mixtures for waste solvent recovery  

Chaniago, Yus Donald (School of Chemical Engineering, College of Engineering, Yeungnam University)
Lee, Moonyong (School of Chemical Engineering, College of Engineering, Yeungnam University)
Publication Information
Journal of Industrial and Engineering Chemistry / v.67, no., 2018 , pp. 255-265 More about this Journal
Abstract
The huge amount of solvents used in the semi-conductor and display industry typically result in waste of valuable solvents which often form complex azeotropic mixtures. This study explored a recovery process of a quaternary waste solvent, comprising methyl 2-hydroxybutyrate, propylene glycol monomethyl ether acetate, ethyl lactate, and ethyl-3-ethoxy propionate. In this study, a novel shortcut column method with a graphical approach was exploited for the distillation column design of complex quaternary azeotropic mixtures. As a result, the proposed shortcut method and design procedure solved the complex separation paths successfully with less computational efforts while achieving all requirements for component purity.
Keywords
Waste solvent recovery; Propylene glycol monomethyl ether acetate; Ethyl lactate; Quaternary azeotropic mixture; Short-cut column method;
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