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Titanium Dioxide Nanofibers Prepared by Using Electrospinning Method  

Ding, Bin (Department of Advanced Organic Materials Engineering, Chonbuk National University)
Kim, Chul Ki (Department of Textile Engineering, Chonbuk National University)
Kim, Hak Yong (Department of Textile Engineering, Chonbuk National University)
Seo, Min Kang (Advanced Materials Division, Korea Research Institute of Chemical Technology)
Park, Soo Jin (Advanced Materials Division, Korea Research Institute of Chemical Technology)
Publication Information
Fibers and Polymers / v.5, no.2, 2004 , pp. 105-109 More about this Journal
Abstract
The synthesis of titanium dioxide nanofibers with 200-300nm diameter was presented. The new inorganic-organic hybrid nanofibers were prepared by sol-gel processing and electrospinning technique using a viscous solution of titanium isopropoxide (TiP)/poly(vinyl acetate) (PVAc). Pure titanium dioxide nanofibers were obtained by high temperature calcination of the inorganic-organic composite fibers. SEM, FT-IR, and WAXD techniques were employed to characterize these nanofibers. The titanium dioxide nanostructured fibers have rougher surface and smaller diameter compare with PVAc/TiP composite nanofibers. The anatase to rutile phase transformation occurred when the calcination temperature was increased from $600^{\circ}C$ to $1000^{\circ}C$.
Keywords
Hybrid nanofibers; Titanium isopropoxide/Poly(vinyl acetate); Titanium dioxide; Calcination;
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