Browse > Article

Quantitative Analysis of Acid Value, Iodine Value and Fatty Acids Content in Vegetable Oils by NIRS  

Kim, Jae-Kwan (Gyeonggi-do Institute of Health and Environment)
Choi, Ok-Kyung (Gyeonggi-do Institute of Health and Environment)
Hwang, Sun-Il (Gyeonggi-do Institute of Health and Environment)
Jeong, Jin-A (Gyeonggi-do Institute of Health and Environment)
Kim, Yun-Sung (Gyeonggi-do Institute of Health and Environment)
Park, Sin-Hee (Gyeonggi-do Institute of Health and Environment)
Son, Mi-Hui (Gyeonggi-do Institute of Health and Environment)
Kwon, Hye-Jung (Gyeonggi-do Institute of Health and Environment)
Lee, Jung-Bock (Gyeonggi-do Institute of Health and Environment)
Kim, Jong-Chan (Gyeonggi-do Institute of Health and Environment)
Publication Information
Journal of environmental and Sanitary engineering / v.22, no.4, 2007 , pp. 65-76 More about this Journal
Abstract
The possibility of rapid quantitative analysis of AV(Acid Value), IV(Iodine Value) and fatty acids in vegetable oils with NIRS(Near-infrared spectroscopy) was evaluated. A calibration equation calculated by MPLS regression technique was developed and correlation coefficient of determination for AV, IV, $C_{16:0},\;C_{18:0},\;C_{18:1},\;C_{18:2},\;C_{18:3},\;and\;C_{20:0}$ content were 0.9727, 0.997, 0.9805, 0.942, 0.9987, 0.9994, 0.9966, and 0.975 respectively. According to the data obtained from validation study, $R^2$ of contents of perilla, corn, soybean, rapaseed oils were 0.897, 0.993, 0.935, 0.707, 0.994, 0.996, 0.984, 0.798, SEP of contents of 0.185, 1.367, 0.899, 0.640, 1.498, 1.360, 0.476, 0.076 by MPLS. The results indicate that the NIRS procedure can potentially be used as a non-destructive analysis method for the rapid and simple measurement of AV, IV and fatty acids in vegetable oils.
Keywords
NIRS; Vegetable oils; AV; IV; Fatty acids;
Citations & Related Records
연도 인용수 순위
  • Reference
1 Kazuhiro Nakamichi,a Ken-Ichiro Suehara, a* Yasuhisa Nakano, a Koii Kakugawa, b Masahiro Tamaic and Takuo Yanoa : Measurement of the concentrations of mannosyl erythritol lipid and soybean oil in the glycolipid fermentation process using near infrared spectroscopy, Journal of Near Infrared Spectroscopy, 10(1), 53-61. 2002   DOI   ScienceOn
2 권용주, 송근섭. 이태규 호박씨의 지방성분에 관한 연구 전북대학교 농업과학기술연구소 농대논문집, 16, pp. 107-114. 1985
3 권경순, 김현구, 안병수 : 일반계 및 다수계 미강유의 지방질 함량과 중성지방질 조성, 한국식품과학회지, 28(2), 207-211. 1996
4 김준한, 곽동윤, 최명숙, 문광덕 :한국산과 중국산 홍화종실의 화학적 성분 비교, 한국 식품과학회지, 31(4), 912-918. 1999
5 신동화, 정종구 :쌀눈 유지의 저장중 변화와 지방산 구성, 한국식품과학회지, 30(1), 77-81. 1998
6 강명화, 류수노, 김진경, 방진기, 이봉호 : 국내 유료작물의 생산과 식용유 수급동향, 한국 국제농업개발학회지, 11(3), 298-306. 1999
7 한국농촌경제연구원. 식품수급표 http://www. krei.re.kr/kor/main.php, 2005
8 . Golebiowski : Near infrared reflectance spectroscopy of oil in intact canola seed (Brass ica napus, L.). I. Attributes of the intact seed spectrum, Journal of Near Infrared Spectroscopy, 12(5), 325-330. 2004   DOI   ScienceOn
9 송재철 : 식품재료학, 교문사, 351-361. 1992
10 황종택, 강한철, 김태수, 박원종 :포도씨의 지방질 조성과 이화학적 특성, 한국식품영양학회지, 12(2), 150-155. 1999
11 김세원, 고영수 :국내 식물성 혼합유의 산화 안정성 및 가열시 이화학적 변화에 관한 연구, 한국생활과학연구, 10, 193-220. 1992
12 A. Jimenez Marquez : Monitoring carotenoid and chlorophyll pigments in virgin olive oil by visible-near infrared transmittance spectroscopy. On-line application, Journal of Near Infrared Spectroscopy, 11(3), 219-226. 2003   DOI   ScienceOn
13 김동훈 : 식품화학, 탐구당, 451-506. 1998
14 김현위, 배수경, 이해순 :국내 유통되는 올리브오일의 품질특성 실태조사, 한국식품과학회지, 35(6), 1064-1071. 2003
15 최기영, 고영수 : 한국산 식물식용유지의 성분에 관한 연구 -제3보 해바라기종자의 유성성분에 대하여- 한국영양학회지, 12(2), 2075-2085. 1979
16 T. Golebiowski, A.S. Leong and J.F.Panozzo : Near infrared reflectance spectroscopy of oil in intact canola seed (Brassica napus L.). II. Association between principal components and oil content, Journal of Near Infrared Spetroscopy 13(5), 255-264. 2005   DOI   ScienceOn
17 홍진환, 최재천, 최현철, 강명희, 최장덕, 양창숙, 김광수, 백성열, 김보경, 오해성, 이희식, 조래광 :근외분광분석법에 의한 옥배유, 팝유, 돈지의 산가, 요오드가, 비누화가 측정, 식품의약품안전청 연보 1, 123-129. 1997
18 Marena Manley* and Kerstin Eberle : Compari son of Fourier transform near infrared spectroscopy partial least square regression models for South African extra virgin dive oil using spectra collected on two spectrophometers at different resolutions and pathlengths, Journal of Near Infrared Spectroscopy, 14(2), 111-126. 2006   DOI   ScienceOn