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Monitoring and Evaluation of Analytical Methods of Perchlorate with IC and LC/MS  

Kim, Hwa-Bin (Department of Environment Engineering, Pusan National University)
Sim, Won-Jin (Department of Environment Engineering, Pusan National University)
Kim, Min-Young (Department of Environment Engineering, Pusan National University)
Oh, Jeong-Eun (Department of Environment Engineering, Pusan National University)
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Abstract
In this study, we tried to establish analysis methods of perchlorate with ion chromatography(IC) and liquid chromatography/mass spectrometry(LC/MS) and monitored perchlorate levels in various kinds of water and soil samples. The obtained method detection limit(MDL) of IC was 1 ppb and that of LC/MS was 0.005 ppb in water sample. We monitored the ground and spring water in Busan and the average perchlorate level in ground water was 0.031 $\pm$ 0.011 ppb and that of spring water was 0.013 $\pm$ 0.014 ppb. Wastewater samples were also examined and the levels of perchlorate ranged from 0.007 to 0.380 ppb. The perchlorate levels in all water samples investigated in this study were below the EPA guideline.
Keywords
Perchlorate; IC; LC-MS; Analysis Method;
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Times Cited By KSCI : 1  (Citation Analysis)
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