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Development of Analytical Method for Polychlorinated Biphenyls and Organochlorine Pesticides in Air  

최민규 (건국대학교 환경공학과)
여현규 (건국대학교 환경공학과)
김태욱 (한경대학교 환경공학과)
천만영 (한경대학교 환경공학과)
선우영 (건국대학교 환경공학과)
Publication Information
Journal of Korean Society for Atmospheric Environment / v.18, no.6, 2002 , pp. 475-485 More about this Journal
Abstract
An analytical method was investigated for the meaiiurement of polychlorinated biphenyls (PCBs) and organochlorine pesticides (OCPs) concentrations in air samples. Procedures required for column chromatographic clean up. silicagel (stage I) and gel permeation chromatography (stage II), were discussed. Identification and quantification of PCBs and OCPs were performed using a combination of gas chromatography/mass spectrometry/ selected ion monitoring. Recovery tests calculated from six samples are 68∼137% for PCBs and 58∼130% for OCPs except for endrin aldehyde. Instrumental detection limits determined for the PCBs and OCPs varied from 0.05 to 0.18 pg/m3 and from 0.71 to 16.82 pg/㎥, respectively. The method has been applied to the analysis of air samples collected at Ansung city, Kyonggi province, Korea. This method may serve as a screening protocol for the simultaneous determination of PCBs and OCPs in air.
Keywords
PCBs; OCPs; air sample; column clean up; recovery; detection limit;
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