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http://dx.doi.org/10.5395/JKACD.2007.32.4.365

THE BONDING DURABILITY OF TOTAL ETCHING ADHESIVES ON DENTIN  

Jung, Mi-Ra (Department of Conservative Dentistry, Division of Dentistry, Graduate of Kyung Hee University)
Choi, Gi-Woon (Department of Conservative Dentistry, Division of Dentistry, Graduate of Kyung Hee University)
Park, Sang-Hyuk (Department of Conservative Dentistry, Division of Dentistry, Graduate of Kyung Hee University)
Park, Sang-Jin (Department of Conservative Dentistry, Division of Dentistry, Graduate of Kyung Hee University)
Publication Information
Restorative Dentistry and Endodontics / v.32, no.4, 2007 , pp. 365-376 More about this Journal
Abstract
The purpose of this study was to evaluate the effect of different etching times on microtensile bond strength (${\mu}TBS$) to dentin both initial and after thermocycling with 3 different types of total-etching adhesives. Fifty four teeth were divided into 18 groups by etching times (5, 15, 25 sec), adhesives types (Scotchbond Multipurpose (SM), Single Bond (SB), One-Step (OS)) and number of thermocycling (0, 2,000 cycles). Flat dentin surfaces were prepared on mid-coronal dentin of extracted third molars. After exposed fresh dentin surfaces were polished with 600-grit SiC papers, each specimen was acid-etched with 35% phosphoric acid (5, 15, 25 sec) and bonded with 3 different types of total etching adhesives respectively. Then, hybrid composite Z-250 was built up. Half of them were not thermocycled (control group) and the ethers were subjected to 2,000 thermocycle (experimental group). They were sectioned occluso-gingivally into $1.0\;{\times}\;1.0\;mm^2$ composite-dentin beams and tested with universal testing machine at a crosshead speed of 1.0 mm/min. Within limited data of this study, the results were as follows 1. There was no statistically significant difference in ${\mu}TBS$ between the thermocycled and non-thermocycled groups, except for both SM and SB etched for 25 sec. 2. In thermocycled SM and SB groups, bond strength decreased by extended etching time. In total etching systems, adhesive durability for dentin could be affected by type of solvents in adhesive and etching time. Especially, extended etching time may cause deteriorate effects on bond strength when ethanol-based adhesive was used.
Keywords
${\mu}TBS$; Etching time; Type of adhesive; Thermocycling; Total-etching systems; Ethanol-based adhesive;
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  • Reference
1 Nakabayashi N, Nakamura M, Yasuda N. Hybrid layer as a dentin-bonding mechanism. J Esthet Dent 3: 133-138, 1991   DOI
2 Gwinnett AJ. Chemically conditioned dentin: A comparison of conventional and environmental SEM finding. Dent Mater 10:150-155, 1994   PUBMED
3 Pashley DH, Horner JA, Brewer PD. Interactions of conditioners on the dentin surface. Oper Dent Suppli 5:137-150, 1992   PUBMED
4 Titley K, Chernecky R. Maric B, Valiquette N, Smith DC. The morphology of the demineralized layer in primed dentin. Am J Dent 7:22-26, 1994   PUBMED
5 Hashimoto M, Ohno H, Sano H, Tay FR, Kaga M, Kudou Y, Oguchi H, Araki Y, Kuboda M. Micromorphological changes in resin-dentin bonds after 1 year water storage. J Biomed Mater Res 63:306-311, 2002   DOI   ScienceOn
6 Koshiro K. Inoue S, Tanaka T, Koase K. Fujita M, Hashimoto M, Sano H. In vivo degradation of resindentin bonds produced by a self-etch vs. a total etch adhesive system. Eur J Oral Sci 112:368-375, 2004   DOI   ScienceOn
7 Gale MS, Darvell BW, Thermal cycling procedure for laboratory testing of dental restorations. J Deht 27:8999, 1999
8 Kubo S, Yokota H, Sata y, Hayashi Y. Microleakage of self-etching primers after thermal and flexural load cycling. Am J Dent 14:163-169, 2001   PUBMED
9 Cardoso PE, Placido E, Moura SK. Microleakage of four simplified adhesive systems under thermal and mechanical stresses. Am J Dent 15: 164-168, 2002   PUBMED
10 Frankenberger R, Kramer N, Petschelt A. Long-term effect of dentin primers on enamel bong strength and marginal adaptation. Oper Dent 25:11-19, 2000   PUBMED
11 Hashimoto M, Ohno H, Sano H, Kaga M, Oguchi H. In vitro degradation of resin-dentin bonds analyzed by microtensile bond test, scanning and transmission electron microscopy. Biomaterials 24:3795-3803, 2003   DOI   ScienceOn
12 Kanca J. Effects of resin primer solvents and surface wetness on resin composite bond strengths to dentin. Am J Dent 5:213-215, 1992   PUBMED
13 Pashley EL. Zhang Y. Lockwood PE. Rueggeberg FA. Pashley DH. Effects of HEMA on water evaporation from water-HEMA mixtures. Dent Mater 14:6-10, 1998   DOI   ScienceOn
14 Mauro FN, Edward JS, Jorge P. Effects of de mineralization depth on microtensile bond strength to human dentin. J Adhes Dent 3: 137-143, 2001   PUBMED
15 Pashely DH. The effect of acid etching on the pulpodentin complex. Oper Dent 17:229-242, 1992   PUBMED
16 Amstrong SR. Keller JC, Boyer DB. The influence of water storage and C-factor on the dentin-resin composite microtensile bond strength and debond pathway utilizing a filled and unfilled adhesive resin. Dent Mater 17:268-276, 2001   DOI   ScienceOn
17 Van Meerbeek B, Inokoshi S, Braem M, Lambrechts P, Vanherle G. Morphological aspects of the resin-dentin interdiffusion zone with different dentin adhesive system. J Dent Res 71: 1530-1540, 1992   DOI   PUBMED   ScienceOn
18 Van Meerbeek B, Vargas M, Inoue S, Yoshida Y, Peumans M, Lambrechts P, Vanherle G. Adhesives and cements to promote preservation dentistry. Oper Dent 26: 119-144, 2001
19 Sano H, Yoshikawa T, Pereira PNR, Kanemura N, Morigami M, Tagami J, Pashley DH. Long-term durability of dentin bonds made with a self etching primer, in vivo. J Dent Res 78:906-911, 1999   DOI   ScienceOn
20 Yoshida Y, Van Meerbeeek B, Nakayama Y, Snauwaert .I, Hellemans L, Lambrechts P, Vanherle G, Wakasa K. Evidence of chemical bonding at biomaterial-hard tissue interfaces. J Dent Res 79: 709-714, 2000   DOI   ScienceOn
21 Camps J, Pashely DH. Buffering action of human dentin in vitro. J Adhes Dent 2:39-50, 2000   PUBMED
22 Titley K, Chernecky R. Maric B, Smith D. Penetration of a dentin bonding agent into dentin. Am J Dent 7: 190-194, 1994   PUBMED
23 Erick JD, Gwinnett AJ. Pashley DH, Robinson SJ. Current concepts on adhesion to dentin. Crit Rev Oral BioI Med 8:306-335, 1997   DOI
24 Uno S, Finger WJ. Effects of acidic conditioners on dentine demineralization and dimension of hybrid layers. J Dent 24:211-216, 1996   DOI   ScienceOn
25 Reis A, Loguercio AD, Azevedo CLN, Carvalho RM, Singer JM, Grande RHM. Moisture spectrum of demineralized dentin for different solvent-based adhesive system. J Adhes Dent 5: 183-192, 2003   PUBMED
26 Sano H. Takatsu T, Ciucchi B, Horner JA, Matthews WG, Pashley DH, Nanoleakage: leakage within the hybrid layer. Oper Dent 20: 18-25, 1995   PUBMED
27 Erickson RL. Surface interactions of dentin adhesive materials. Oper Dent 5: 81-94, 1992   PUBMED
28 Tay FR. Gwinnett JA, Wei SH. Relation between water content in acetone/alcohol-basd primer and interfacial ultrastructure. J Dent 26:147-156, 1998   DOI   ScienceOn
29 Van Meerbeek B, Yoshida Y, Lambrechts P, Vanherle G, Duke ES, Eick JD, Robinson SJ. TEM study of two water-based adhesive systems bonded to dry and wet dentin. J Dent Res 77:50-59, 1998   DOI   ScienceOn
30 De Munck J, Van Meerbeek B, Yoshida Y, Inoue S, Vargas M, Suzuki K. Lanbrechts P, Vanherle G. Four year water degradation of total-etch adhesives bonded to dentin. J Dent Res 82: 136-140, 2002
31 Amer AH, Valeria VG. Evaluation of etching time on dentin bond strength using single bottle bonding systems. J Adhes Dent 6:105-110, 2004   PUBMED
32 Gwinnett AJ, Yu S. Effect of long-term water storage on dentin bonding. Am J Dent 8:109-111, 1995   PUBMED
33 Alessandra R, Alessandro DL, Ricardo Me, Rosa HM. Durability of resin dentin interfaces: effects of surface moisture and adhesive solvent component. Dent Mater 20: 669-676, 2004   DOI   ScienceOn
34 Mjor lA, Moorhead JE, Dahl JE. Reasons for replacement of restorations in permanent teeth in general dental practice. Int Dent J 50:360-366, 2000
35 Kinney JH, Balooch M, Hauot .JrDI, Marshall SJ, Marshall JrGW. Mineral distribution and dimensional changes in human dentin during demineralization. J Dent Res 74:1179-1184, 1995   DOI   ScienceOn
36 Hashimoto M, Ohno H, Kaga M, Kudo K. Sano H, Oguchi H. In vivo degradation of resin-dentin bonds in humans over 1 to 3 years. J Dent Res 79: 1385-1391. 2000   DOI   ScienceOn
37 Paul SJ, Leach M, Rueggeberg FA, Pashley DH. Effect of water content on the physical properties of model dentine primer and bonding resins. J Dent 27: 209-214, 1999   DOI   ScienceOn
38 Inokoshi S, Hosoda H. Harnirattisai C, Shimada Y. Interfacial structure between dentin and seven dentin bonding systems revealed using argon ion beam etching. Oper Dent 18:8-16, 1993   PUBMED
39 Carvalho RM, Mendonca JS, Santiago SL, Silveira RR. Garcia FCP, TayFR, Pashley DH. Effects of HEMA/solvent combinations on bond strength to dentin. J Dent Res 82:597-601. 2003   DOI   ScienceOn
40 Amer A, Valeria V. Evaluation of etching time on dentin bond strength using single bottle bonding systems. J Adhes Dent 6:105-110, 2004   PUBMED
41 Giannini M, Seixas CAM, Reis AF, Pimenta LAF. Six-month storage-time evaluation of one-bottle adhesive systems to dentin. J Esth Rest Dent 15:43-8, 2003   DOI   ScienceOn