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http://dx.doi.org/10.4047/jap.2013.5.4.464

Degree of conversion of two dual-cured resin cements light-irradiated through zirconia ceramic disks  

Kim, Min-Jeong (Department of Medical & Biological Engineering, Graduate School, Kyungpook National University)
Kim, Kyo-Han (Department of Dental Biomaterials, School of Dentistry, and Institute for Biomaterials Research & Development, Kyungpook National University)
Kim, Young-Kyung (Department of Conservative Dentistry, School of Dentistry, Kyungpook National University)
Kwon, Tae-Yub (Department of Dental Biomaterials, School of Dentistry, and Institute for Biomaterials Research & Development, Kyungpook National University)
Publication Information
The Journal of Advanced Prosthodontics / v.5, no.4, 2013 , pp. 464-470 More about this Journal
Abstract
PURPOSE. The aim of this Fourier transform infrared (FTIR) spectroscopic study was to measure the degree of conversion (DC) of dual-cured resin cements light-irradiated through zirconia ceramic disks with different thicknesses using various light-curing methods. MATERIALS AND METHODS. Zirconia ceramic disks (KT12) with three different thicknesses (1.0, 2.0, and 4.0 mm) were prepared. The light transmittance of the disks was measured using ultraviolet visible near-infrared spectroscopy. Four different light-curing protocols were used by combining two curing light modes (Elipar TriLight (standard mode) and bluephase G2 (high power mode)) with light-exposure times of 40 and 120 seconds. The DCs of the two dual-cured resin cements (Duo-Link and Panavia F2.0) light-irradiated through the disks was analyzed at three time intervals (3, 7, and 10 minutes) by FTIR spectroscopy. The data was analyzed using repeated measures ANOVA (${\alpha}$=.05).Two-way ANOVA and Tukey post hoc test were used to analyze the 10 minute DC results. RESULTS. The 1.0 mm thick disk exhibited low light transmittance (<25%), and the transmittance decreased considerably with increasing disk thickness. All groups exhibited significantly higher 10 minute DC values than the 3 or 7 minute values (P<.05), but some exceptions were observed in Duo-Link. Two-way ANOVA revealed that the influence of the zirconia disk thickness on the 10 minute DC was dependent on the light-curing methods (P<.001). This finding was still valid even at 4.0 mm thickness, where substantial light attenuation took place. CONCLUSION. The curing of the dual-cured resin cements was affected significantly by the light-curing technique, even though the additional chemical polymerization mechanism worked effectively.
Keywords
Resin cement; Zirconia ceramic; Degree of conversion;
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