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http://dx.doi.org/10.4150/KPMI.2011.18.3.277

Synthesis of LiCoO2 Powders using Recycled Cobalt Precursors from Waste WC-Co Hard Metal  

Yang, Hee-Seung (Engineering Ceramic Center, Korea Institute of Ceramic Engineering and Technology)
Pee, Jae-Hwan (Ceramicware Technology Center, Korea Institute of Ceramic Engineering and Technology)
Kim, Yoo-Jin (Engineering Ceramic Center, Korea Institute of Ceramic Engineering and Technology)
Publication Information
Journal of Powder Materials / v.18, no.3, 2011 , pp. 277-282 More about this Journal
Abstract
[ $LiCoO_2$ ] a cathode material for lithium rechargeable batteries, was prepared using recycled $Co_3O_4$. First, the cobalt hydroxide powders were separated from waste WC-Co hard metal with acid-base chemical treatment, and then the impurities were eliminated by centrifuge method. Subsequently, $Co_3O_4$ powders were prepared by thermal treatment of resulting $Co(OH)_2$. By adding a certain amount of $Li_2CO_3$ and $LiOH{\cdot}H_2O$, the $LiCoO_2$ was obtained by sintering for 10 h in air at $800^{\circ}C$. The synthesized $LiCoO_2$ particles were characterized by X-ray diffraction (XRD) and Scanning Electron Microscope (SEM) analysis.
Keywords
WC-Co composite powder; Recycle; Cobalt oxide; Lithium cobalt oxide;
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