Browse > Article
http://dx.doi.org/10.4150/KPMI.2010.17.3.223

Fabrication of Iron-Molybdenum Alloyed Nanoparticle and Nanowire using Chemical Vapor Condensation(CVC)  

Ha, Jong-Keun (School of Materials Science and Engineering, i-cube Center & ERI, Gyeongsang National University)
Cho, Kwon-Koo (School of Materials Science and Engineering, i-cube Center & ERI, Gyeongsang National University)
Kim, Ki-Won (School of Materials Science and Engineering, i-cube Center & ERI, Gyeongsang National University)
Ryu, Kwang-Sun (Department of Chemistry, University of Ulsan)
Publication Information
Journal of Powder Materials / v.17, no.3, 2010 , pp. 223-229 More about this Journal
Abstract
Iron(Fe)-Molybdenum(Mo) alloyed nanoparticles and nanowires were produced by the chemical vapor condensation(CVC) process using the pyrolysis of iron pentacarbonyl($Fe(CO)_5$) and Molybdenum hexacarbonyl($Mo(CO)_6$). The influence of CVC parameter on the formation of nanoparticle, nanowire and size control was studied. The size of Fe-Mo alloyed nanoparticles can be controlled by quantity of gas flow. Also, Fe-Mo alloyed nanowires were produced by control of the work chamber pressure. Moreover, we investigated close correlation of size and morphology of Fe-Mo nanoparticles and nanowires with atomic quantity of inflow precursor into the electric furnace as the quantitative analysis. Obtained nanoparticles and nanowires were investigated by field emission scanning electron microscopy, energy dispersive spectroscopy and X-ray diffraction.
Keywords
Chemical vapor condensation; Fe-Mo; Alloy; Nanoparticles; Nanowires;
Citations & Related Records
연도 인용수 순위
  • Reference
1 G. H. Lee, S. H. Huh, J. W. Jeong and H.-C. Ri: J. Magn. Mater., 246 (2002) 404.   DOI   ScienceOn
2 C. J. Choi, O. Tolochko and B. K. Kim: Materials Letters,56 (2002) 289.   DOI   ScienceOn
3 X. L. Dong, C. J. Choi and B. K. Kim: Scripta Mater.,47 (2002) 857.   DOI   ScienceOn
4 W. Chang, G. Skandan, H. Hahn, S. C. Danforth andB. K. Kear: Nanostruct. Mater., 4 (1994) 345.   DOI   ScienceOn
5 V. G. Syrkin and Poroshkovaya Metallurgiya: Poroshkovaya Metall- urgiya, 3 (1963) 75.
6 Zhiquan Jiang, Weixin Huang, Jian Jiao, Hong Zhao,Dali Tan, Runsheng Zhai and Xinhe Bao: Applied Surface Sci., 229 (2004) 43.   DOI   ScienceOn
7 Menachem Motiei, Jose Calderon Moreno and AharonGedanken: Chem. Phy. Lett., 357 (2002) 271.
8 J-K. Ha, K.-K. Cho, K.-W. Kim, T.-H. Nam, H.-J. Ahnand G.-B. Cho: Mater. Sci. Forum, 534-536 (2007) 29.   DOI
9 C. G. Granqvist and R. A. Buhrman: Solid State Communications.,18 (1976) 123.   DOI   ScienceOn
10 C. J. Choi, X. L. Dong and B. K. Kim: Scripta mater.,44 (2001) 2225.   DOI   ScienceOn
11 G. Skandan, Y.-J Chen, N. Glumac, and B. H. Kear:Nanostruct. Mater., 11 (1999) 149.   DOI   ScienceOn
12 G. F. Gaertner and H. Lydtin: Nanostruct. Mater., 4 (1994) 559.   DOI   ScienceOn
13 L. Savinia, E. Bonettia, L. Del Biancoa, L. Pasquinia,L. Signorinia, M. Coissonb and V. Selvagginic: J. Magn. Mater., 262 (2003) 56.   DOI   ScienceOn
14 S. H. Huh, H. K. Kim, J .W. Park and G. H. Lee: Phys. Rev. B, 62 (2000) 2937.   DOI   ScienceOn
15 L. Savini, E. Bonetti, L. Del Bianco, L. Pasquini, L.Signorini, M. Coisson and V. Selvaggini: J. Magn. Mater., 262 (2003) 56.   DOI   ScienceOn