Browse > Article
http://dx.doi.org/10.7234/composres.2016.29.6.408

Manufacturing and Mechanical Properties of Epoxy Fibers Spinning using Anhydride and Amine Hardeners  

Shin, Pyeong-Su (Department of Materials Engineering and Convergence Technology, Center for Creative Human Resource & Convergence Materials, Research Institute for Green Energy Convergence Technology, Gyeongsang National University)
Kim, Jong-Hyun (Department of Materials Engineering and Convergence Technology, Center for Creative Human Resource & Convergence Materials, Research Institute for Green Energy Convergence Technology, Gyeongsang National University)
Park, Ha-Seung (Department of Materials Engineering and Convergence Technology, Center for Creative Human Resource & Convergence Materials, Research Institute for Green Energy Convergence Technology, Gyeongsang National University)
Baek, Yeong-Min (Department of Materials Engineering and Convergence Technology, Center for Creative Human Resource & Convergence Materials, Research Institute for Green Energy Convergence Technology, Gyeongsang National University)
Kwon, Dong-Jun (Department of Materials Engineering and Convergence Technology, Research Institute for Green Energy Convergence Technology, Gyeongsang National University)
Park, Joung-Man (Department of Materials Engineering and Convergence Technology, Research Institute for Green Energy Convergence Technology, Gyeongsang National University)
Publication Information
Composites Research / v.29, no.6, 2016 , pp. 408-413 More about this Journal
Abstract
Commonly-used polymers are manufactured as versatile forms. Furthermore, continuous polymer fibers are recently manufactured using nylon or aramid fiber. One of common epoxy was also used to make polymer fibers. Bisphenol-A type was used as base epoxy whereas amine and anhydride were used as hardeners. Epoxy fibers was cured by stepping up the temperature to maintain the shape of epoxy fiber. Surface energy was measured to confirm the degree of interfacial adhesion by modified static contact angle method. After mechanical properties were measured via fiber tensile test, the evaluation of fiber fracture was proceeded. Tensile strength of epoxy fiber using amine type hardener was higher as 138 MPa than anhydride case as 70 MPa. Fractured surface exhibited different failure patterns at the cross-section.
Keywords
Epoxy fiber; Acid anhydride; Amine; Hardener; Micro crack;
Citations & Related Records
연도 인용수 순위
  • Reference
1 Hufenus, R., Gottardo, L., Leal, A.A., Zemp, A., Heutschi, K., Schuetz, P., Meyer, V.R., and Heuberger, M., "Melt-Spun Polymer Fibers with Liquid Core Exhibit Enhanced Mechanical Damping," Materials & Design, Vol. 110, 2016, pp. 685-692.   DOI
2 Li, D., Wu, D., Yang, Z., Zhou, Y., Wang, S., Duan, X., Jia, D., Zhu, Q., and Zhou, Y., "Effects of in situ Amorohour Graphite Coating on Ablation Resistance of SiC Fiber Reinforced SiBCN Ceramics in an Oxyacetylene Flame," Corrosion Science, Vol. 113, 2016, pp. 31-45.   DOI
3 Wang, J., Duan, X., Yang, Z., Jia, D., and Zhou, Y., "Ablation Mechanism and Properties of SiCf/SiBCN Ceramic Composites under an Oxyactylene Torch Environment," Corrosion Science, Vol. 82, 2014, pp. 101-107.   DOI
4 He, z., Xuan, H., Bai, C.., Hu, Y., Cong, P., Bai, H., Miao, Y., and Hong, W., "Containment Tests and Analysis of Soft Wall Casing Fabricated by Wrapping Kevlar Fabric Around Thin Metal Ring," Aerospace Science and Technology, Vol. 61, 2017, pp. 35-44.   DOI
5 Sharafi, S., and Li, G., "Multiscale Modeling of Vibration Damping Response of Shape Memory Polymer Fibers," Composites Part B, Vol. 91, 2016, pp. 306-314.   DOI
6 Zhang, W., Xue, Z., Yan, M., Liu, J., and Xia, Y., "Effect of Epichlorohydrin on the Wet Spinning of Carrageenan Fibersunder Optimal Parameter Conditions," Carbohydrate Polymers, Vol. 150, 2016, pp. 232-240.   DOI
7 Sharafi, S., and Li, G., "Multiscale Modeling of Vibration Damping Response of Shape Memory Polymer Fibers," Composites Part B, Vol. 91, 2016, pp. 306-314.   DOI
8 Yang, W., Bin, Y., Yuan, Y., and Matsuo, M., "Evaluation for Most Probable Distance between Adjacent Amorphous Molecular Chains Taking Preferred Orientation with Respect to a Spinning Fiber," Polymer, Vol. 103, 2016, pp. 112-123.   DOI
9 Stajanca, P., Cetinkaya, O., Schukar, M., Mergo, P., Webb, D.J., and Krebber, K., "Molecular Alignment Relaxation in Polymer Optical Fibers for Sensing Applications," Optical Fiber Technology, Vol. 28, 2016, pp. 11-17.   DOI
10 Li, D., Chen, W., Sun, B., Li, H., Wu, T., Ke, Q., Huang, C.., Ei-Hamshary, H., Al-Deyab, S.S., and Mo, X., "A Comparison of Nanoscale and Multiscale PCL/Gelatin Scaffolds Prepared by Disc-Electro spinning," Colloids and Surface B: Biointerfaces, Vol. 146, 2016, pp. 632-641.   DOI
11 Ahmed, D., Hongpeng, Z., Haijuan, K., Jing, L., Yu, M., and Muhuo, Y., "Microstructural Developments of Poly (p-phenylene terephthalamide) Fibers During Heat Treatment Process: A Review," Materials Research, 2014, Vol. 7, pp. 1180-1200.
12 Chen, R.S., Ahmad, S., Gan, S., Salleh, M.N., Ghani, M.H.A., and Tarawneh, M.A., "Effect of Polymer Blend Matrix Compatibility and Fibre Reinforcement Content on Thermal Stability and Flammability of Ecocomposites Made from Waste Materials," Thermochimica Acta, Vol. 640, 2016, pp. 52-61.   DOI
13 Fang, H., Zhang, Y., Deng, J., and Rodrigue, D., "Effect of Fiber Treatment on the Water Absorption and Mechanical Properties of Hemp Fiber/Polyethylene Composites," Journal of Applied Polymer Science, Vol. 127, 2013, pp. 942-949.   DOI