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http://dx.doi.org/10.5806/AST.2012.25.6.435

Determination of perchlorate in the Gum-River surface water by LC-ESI-MS/MS  

Lee, Young Joon (Geum River Environment Research Center, National Institute of Environmental Research)
Lee, Jun Bae (Geum River Environment Research Center, National Institute of Environmental Research)
Hong, Seon Haw (Geum River Environment Research Center, National Institute of Environmental Research)
Kim, Hyun-Ji (Department of Environmental Science, Kongju National University)
Shin, Ho-Sang (Department of Environmental Education, Kongju National University)
Publication Information
Analytical Science and Technology / v.25, no.6, 2012 , pp. 435-440 More about this Journal
Abstract
A liquid chromatography-electrospray ionization-tandem mass spectrometry method (LC-ESI-MS/MS) was used for determining perchlorate in the Gum-River surface water. Sample was directly injected into LC-ESI-MS/MS after the filtrations using PTFE filter paper. The coefficient of variation of perchlorate was less than 3% and the limit of quantification was 0.17 ${\mu}g/L$. Water samples were collected from thirty-five basins of Gum-River on February, April and June 2012, respectively. As a result, perchlorate was detected in the concentration range of 0.23-3.73 ${\mu}g/L$ (mean 0.20 ${\mu}g/L$) in the frequency of 15% in general surface water and in the concentration range of 0.36-25.10 ${\mu}g/L$ (mean 1.69 ${\mu}g/L$) in the frequency of 36% in surface water samples near industry area.
Keywords
LC-ESI-MS/MS; perchlorate; surface water; trace analysis;
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1 Wikipedia encyclopedia, http://en.wikipedia.org/wiki/Perchlorate, Last accessed on 25 July 2012.
2 E. T. Urbansky, Biorem. J., 2, 81-95 (1998).   DOI   ScienceOn
3 E. T. Urbansky and M. R. Schock, J. Environ. Manage., 56, 79-95 (1999).   DOI   ScienceOn
4 W. E. Motzer, Environ. Forensics, 2, 301-311 (2001).   DOI   ScienceOn
5 H. P. Wagner, B. V. Pepich, C. Pohl, D. Later, R. Joyce, K. Srinivasan, D. Thomas, A. Woodruff, B. DeBorba and D. J. Munch, J. Chromatogr. A, 1118(1), 85-93 (2006).   DOI   ScienceOn
6 A. B. Kirk, P. K. Martinelango, K. Tian, A. Dutta, E. E. Smith and P. K. Dasgupta, Environ. Sci. Technol., 39(7), 2011-2017 (2005).   DOI   ScienceOn
7 J. V. Dyke, K. Ito, T. Obitsu, Y. Hisamatsu, P. K. Dasgupta and B. C. Blount, Environ. Sci. Technol., 41(1), 88-92 (2007).   DOI   ScienceOn
8 Y. Li and E. J. George, Anal. Chem., 77(14), 4453-4458 (2005).   DOI   ScienceOn
9 S. C. Wendelken, L. E. Vanatta, D. E. Coleman and D. J. Munch, J. Chromatogr. A, 1118(1), 94-99 (2006).   DOI   ScienceOn
10 S. A. Snyder, B. J. Vanderford and D. J. Rexing, Environ. Sci. Technol., 39(12), 4586-4593 (2005).   DOI   ScienceOn
11 Y. Shi, P. Zhang, Y. Wang, J. Shi, Y. Cai, S. Mou and G. Jiang, Environ. Int., 33(7), 955-962 (2007).   DOI   ScienceOn
12 R. T. Wilkin, D. D. Fine and N. G. Burnett, Environ. Sci. Technol., 41(11), 3966-3971 (2007).   DOI   ScienceOn
13 C. J. Koester, H. R. Beller and R. U. Halden, Environ. Sci. Technol., 34(9), 1862-1864 (2000).   DOI   ScienceOn
14 M. A. Greer, G. Goodman, R. C. Pleus and S. E. Greer, Environ. Health Perspect., 110(9), 927-937 (2002).   DOI
15 M. L. Magnuson, E. T. Urbansky and C. A. Kelty, Anal. Chem., 72(1), 25-29 (2000).   DOI   ScienceOn
16 A. Srinivasan and T. Viraraghavan, Int. J. Environ. Res. Public Health, 6(4), 1418-1442 (2009).   DOI
17 R. E. Tarone, L. Lipworth and J. K. McLaughlin, J. Occup. Environ. Med., 52(6), 653-660 (2010).   DOI   ScienceOn
18 U.S. Environmental Protection Agency, Fact Sheet: Final Third Contamination Candidate List (CCL3), EPA Document No. 815-F-09-001, Washington, DC, September 2009.
19 U.S. Environmental Protection Agency, Interim Drinking Water Health Advisory for Perchlorate, EPA Document No. 822-R-08-025, Washington, DC, December 2008.
20 U.S. Environmental Protection Agency, Contaminant Information Sheets for the Final CCL3 Chemicals, EPA Document No. 815-R-09-012, Washington, DC, August 2009.
21 U.S. Environmental Protection Agency, Drinking Water: Preliminary Regulatory Determination on Perchlorate, EPA Document No. EPA-HQ-OW-2008-0692, Washington, DC, October 2008.
22 M. A. Mazloum, M. Jalayer and H. Naeimi, Anal. Bioanal. Chem., 381(6), 1186-1192 (2005).   DOI
23 S. V. Khimchenko, L. P. Eksperiandova and A. B. Blank, J. Anal. Chem., 64(1), 14-17 (2009).   DOI
24 N. Pourreza and H. Z. Mousavi, J. Anal. Chem., 60(9), 816-818 (2005).   DOI
25 G. Soledad, A. Isabel, A. O. Joaquyn, S-P. Concepcion and E. Rosario, Microchim. Acta, 143(1), 59-63 (2003).   DOI
26 A. A. Ensafi and B. Rezaei, Analytical letters, 31(1), 167-177 (1998).   DOI   ScienceOn
27 D. B. Thorburn, M. D. Dunford and P. Sutthivaiyakit, Anal. Chim. Acta, 356(2/3), 141-143 (1997).   DOI   ScienceOn
28 V. S. Hatzistavros and N. G. Kallithrakas-Kontos, Anal. Chem., 83(9) 3386-3391 (2011).   DOI   ScienceOn
29 J. C. Gertsch, S. D. Noblitt and D. M. Cropek, Anal. Chem., 82(9), 3426-3429 (2010).   DOI   ScienceOn
30 I. K. Kiplagat, T. K. Doan and P. Kub, Electrophoresis, 32(21), 3008-3015 (2011).   DOI   ScienceOn
31 X. A. Li, D. M. Zhou and J. J. Xu, Talanta, 75(1), 157- 162 (2008).   DOI   ScienceOn
32 A. V. Pirogov, A. V. Yurev and O. A. Shpigun, J. Anal. Chem., 58(8), 781-784 (2003).   DOI
33 Y. Liu and S. Mou, J. Chromatogr. A, 997(1/2), 225- 235 (2003).   DOI   ScienceOn
34 H. Huang and G. A. Sorial, Chemosphere, 64(7), 1150- 1156 (2006).   DOI   ScienceOn
35 J. D. Lamb, D. Simpson and B. D. Jensen, J. Chromatogr. A, 1118(1), 100-105 (2006).   DOI   ScienceOn
36 L. Barron, P.N. Nesterenko and B. Paull, Anal. Chim. Acta, 567(1), 127-134 (2006).   DOI   ScienceOn
37 P. E. Jackson, M. Laikhtman and J. S. Rohrer, J. Chromatogr. A, 850(1/2), 131-135 (1999).   DOI   ScienceOn
38 K. Tian, P. K. Dasgupta and T. A. Anderson, Anal. Chem., 75(3), 701-706 (2003).   DOI   ScienceOn
39 Y. Liu, S. Mou and S. Heberling, J. Chromatogr. A, 956(1/2), 85-91 (2002).   DOI   ScienceOn
40 P. E. Jackson, S. Gokhale and T. Streib, J. Chromatogr. A, 888(1/2), 151-158 (2000).   DOI   ScienceOn
41 H. C. Chen, W. T. Chen and W. H. Ding, Talanta, 79(2), 442-445 (2009).   DOI   ScienceOn
42 M. L. Magnuson, E. T. Urbansky and C. A. Kelty, Talanta, 52(2), 285-291 (2000).   DOI   ScienceOn
43 E. Hedrick and D. Munch, J. Chromatogr. A, 1039(1/2), 83-88 (2004).   DOI   ScienceOn
44 B. Ells, D. A. Barnett and R. W. Purves, J. Environ. Monit., 2(5), 393-397 (2000).   DOI   ScienceOn
45 R. Handy D. A. Barnett and R. W. Purves, J. Anal. At. Spectrom., 15(8), 907-911 (2000).   DOI   ScienceOn
46 M. L. Magnuson, E. T. Urbansky and C. A. Kelty, Anal. Chem., 72(1), 25-29 (2000).   DOI   ScienceOn
47 S. L. Lin, C. Y. Lo and M. R. Fuh, J. Chromatogr. A, 1246, 40-47 (2012).   DOI   ScienceOn
48 S. M. Backus, P. Klawuun and S. Brown, Chemosphere, 61(6), 834-843 (2005).   DOI   ScienceOn
49 H. B. Kim, J. E. Oh, S. Y. Lee, J. W. Cho and S. Snyder, J. KSEE., 28(7), 776-781 (2006).
50 H. H. Kim, I. S. Han, G. J. Jeong, H. Park, S. H. Han and W. S. Cho, J. KSEE., 32(4), 349-356 (2010).
51 C. A. SANCHEZ, R. I. KRIEGER, N. KHANDAKER, R. C. MOORE, K. C. HOLTS and L. L. NEIDEL, J. Agric. Food. Chem., 53, 5479-5486 (2005).   DOI   ScienceOn
52 K. Kosaka, M. Asami, Y. Matsuoka, M. Kamoshita and K. Shoichi, Water Res, 41, 3474-3482 (2007).   DOI   ScienceOn