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http://dx.doi.org/10.5806/AST.2011.24.4.266

The rapid determination of PAHs in foods using ultra high performance liquid chromatography  

Ha, Jae-Ho (Food Analysis Center, Korea Food Research Institute)
Shin, Dong-Bin (Food Analysis Center, Korea Food Research Institute)
Hwang, Jin-Bong (Food Analysis Center, Korea Food Research Institute)
Seo, Hye-Young (World Institute of Kimchi, An Annex of Korea Food Research Institute)
Ito, Masahito (Hitachi High-Technologies Corp.)
Nakagawa, Hiroaki (Hitachi High-Technologies Corp.)
Publication Information
Analytical Science and Technology / v.24, no.4, 2011 , pp. 266-274 More about this Journal
Abstract
Using a Hitachi LaChrom Ultra 2000U, a reverse phase ultra high performance liquid chromatography (u-HPLC) method was developed for the rapid quantification of 14 PAHs in foods. The proposed method for PAH analysis is based on solid phase extraction (SPE) cartridges; the determination was carried out by u-HPLC with fluorimetric detection. The method was very sensitive; PAH concentration levels were in a low ${\mu}g$/kg range and could be detected and quantified. Six samples of food were analyzed. Among PAHs, PHE was found in most of samples, the concentration ranging from 2.5 to 19.9 ${\mu}g$/kg. The contents of benzo[c]fluorine (BCL), pyrene (PYR), benzo[a]anthracene (BaA), chrysene (CHR), benzo[b]fluoranthene (BbF), benzo[k]fluoranthene (BkF) were low at the '${\mu}g$/kg' level or were less than LOD.
Keywords
UHPLC; rapid analysis; PAHs;
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1 M. S. Garcia-Falcon, B. Cancho-Grande and J. Simal-Gandara, Food Chem., 90, 643-647 (2005).   DOI   ScienceOn
2 A. Stolyhwo and Z. E. Sikorski, Food Chem., 91, 303-311 (2005).   DOI   ScienceOn
3 V. H. Teixeira, S. Casal and M. B. P. P Oliveira, Food Chem., 104, 106-112 (2007).   DOI   ScienceOn
4 G. Purcaro, S. Moret and L. S. Conte, J. Sep. Sci., 31, 3936-3944 (2008).   DOI   ScienceOn
5 M. Suchanova, J. Hajslova, M. Tomaniova, V. Kocourek and L. Babicka, J. Sci. Food Agric., 88, 1307-1317 (2008).   DOI   ScienceOn
6 B. H. Chen and Y. S. Lin, J. Agric. Food Chem., 45, 1394-1403 (1997).   DOI   ScienceOn
7 R. WeiB Haar, Eur. J. Lipid Sci. Technol., 104, 282-285 (2002).   DOI   ScienceOn
8 D. Luo, Q. W. Yu, H. R. Yin and Y. Q. Feng, Anal. Chim. Acta., 588, 261-267 (2007).   DOI   ScienceOn
9 M. Gfrerer and E. Lankmayr, J. Sep. Sci., 26, 1230-12367 (2003).   DOI   ScienceOn
10 N. Kishikawa, M. Wada, N. Kuroda, S. Akiyama and K. Nakashima, J. Chromatogr. B., 789, 257-264 (2003).   DOI   ScienceOn
11 G. Purcaro, S. Moret and L. S. Conte, J. Chromatogr. A., 1176, 231-235 (2007).   DOI   ScienceOn
12 J. Ha, Y. Shim, H. Y. Seo, H. J. Nam, M. Ito and H. Nakagawa, Food Sci. Biotechnol., 19, 1199-1204 (2010).   과학기술학회마을   DOI   ScienceOn
13 S. Moret, G. Purcargo and L. S. Conte, Eur. J. Lipid Sci. Technol., 107, 488-496 (2005).   DOI   ScienceOn
14 B. H. Chen, C. Y. Wang and C. P. Chiu, J. Agric. Food Chem., 44, 2244-2251 (1996).   DOI   ScienceOn
15 S. Moret and L. S. Conte, J. Sep. Sci., 25, 96-100 (2002).   DOI   ScienceOn
16 S. Hu, M. Kim, N. S. Oh, J. Ha, K. S. Choi, K. S. Kwon, Hanguk Sikpum Kwahakhoechi., 37, 866-872 (2005).   과학기술학회마을
17 S. Hu, N. S. Oh, S. Y. Kim and H. Lee, Anal. Sci. Technol., 19, 415-421 (2006).   과학기술학회마을
18 S. Hu, H. Lee, Y. Chae and E. You, Anal. Sci. Technol., 18, 403-409 (2005).   과학기술학회마을
19 M. N. Nayali-Sayadi, S. Rubio-Barroso, M. P. Cuesta-Jimenez and L. M. Polo-Diez, Analyst. 123, 2145-2148 (1998).   DOI   ScienceOn
20 S. Wretling, A. Eriksson, G. A. Eskhult and B. Larsson, J. Food Compos. Anal., 23, 264-272 (2010).   DOI   ScienceOn
21 J. Ha, H. Y. Seo, Y. Shim, H. Seog, M. Ito and H. Nakagawa, J. AOAC Int., 93, 1905-1911 (2010).