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http://dx.doi.org/10.5806/AST.2010.23.2.128

Analytical method of New POPs in environmental samples  

Shin, Sun-Kyoung (National Institute of Environmental Research of Environmental Research)
Park, Jin-Soo (National Institute of Environmental Research of Environmental Research)
Kang, Young-Yeul (National Institute of Environmental Research of Environmental Research)
Lee, Su-Young (National Institute of Environmental Research of Environmental Research)
Chun, Jin-Won (National Institute of Environmental Research of Environmental Research)
Kim, Dong-Hoon (National Institute of Environmental Research of Environmental Research)
Yeon, Jin-Mo (National Institute of Environmental Research of Environmental Research)
Publication Information
Analytical Science and Technology / v.23, no.2, 2010 , pp. 128-137 More about this Journal
Abstract
The purpose of this study is to set up the analytical method of new persistent organic pollutants (POPs) such as chlordecone, endosulfan, ${\alpha}$-HCH, ${\beta}$-HCH, ${\gamma}$-HCH. The analytical methods for these compounds listed as new POPs by the Stockholm Convention need to be newly established. Therefore, we proposed the analytical method for 5 organic chlorinated pesticides (OCPs) and then applied the analytical method to environmental samples. To do this, the pre-treatment such as florisil and activated carbon cleanup process in the Korean official method for classic POPs had been reviewed. All of compounds except chlordecone were pre-treated simultaneously with reviewed cleanup process and detected by GC/MS and HRGC/HRMS respectively. There is a problem that chlordecone could not get a high sensitivity by GC analysis, but in this study GC/MS method was proposed.
Keywords
New POPs; HCH; endosulfan; chlordecone; GC/MS; HRGC/HRMS;
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