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Analytical method of PCDDs/PCDFs in blood using NIST SRM 1589a  

Shin, Sun Kyoung (National Institute of Environmental Research)
Park, Seok Un (National Institute of Environmental Research)
Kim, Tae Seung (National Institute of Environmental Research)
Publication Information
Analytical Science and Technology / v.18, no.6, 2005 , pp. 559-567 More about this Journal
Abstract
For the analytical method of PCDD/Fs in blood, which have been issued recently, SRM 1589a of NIST(National Institute of Standards and Technology) was used and a practical analytical method of PCDD/Fs in blood was presented through comparison of methods of Canada and Japan. The proposed method used alkali-digestion extraction for removal of the lipid effectively using two capillary columns. The limit of quantification of TeCDD/DF and PeCDD/DF was 1 pg/g-lipid, HxCDD/DF and HpCDD/DF was 2 pg/g-lipid, OCDD/DF was 4 pg/g-lipid. With consideration the range of detected concentration, calibration standards were presented as $CS_L$(0.1~1), $CS_1/2$(0.25~2.5), $CS_1$(0.5~5.0), $CS_2$(2~20), $CS_3$(10~100).
Keywords
Serum; PCDDs/PCDFs; Analytical Method; SRM;
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