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Process Parameter Control of Arc Melting Process for Ti3SiC2 MAX Phase Synthesis

Ti3SiC2 MAX Phase 합성을 위한 Arc Melting 공정 제어

  • Nou, Chang Wan (School of Energy, Materials and Chemical Engineering, Korea University of Technology and Education) ;
  • Kim, Byeong Guen (Vehicle Engineering Team, Research Development Division, Gyeongbuk Institute of IT Convergence Industry Technology) ;
  • Bae, Sang Hyun (School of Energy, Materials and Chemical Engineering, Korea University of Technology and Education) ;
  • Choi, Soon-Mok (School of Energy, Materials and Chemical Engineering, Korea University of Technology and Education)
  • 노창완 (한국기술교육대학교 에너지신소재화학공학부) ;
  • 김병근 (경북IT융합산업기술원 연구개발부 차량연구팀) ;
  • 배상현 (한국기술교육대학교 에너지신소재화학공학부) ;
  • 최순목 (한국기술교육대학교 에너지신소재화학공학부)
  • Received : 2020.09.12
  • Accepted : 2020.10.15
  • Published : 2020.11.01

Abstract

The Ti3SiC2 MAX phase was synthesized by arc-melting process under three different processing times. We confirmed that the reaction between the TiCX phase and Ti-Si liquid phase is important for the synthesis of the Ti3SiC2 MAX phase. Results suggest that the Ti3SiC2 MAX phase decomposed when the arc-melting time was greater than 80s. Herein, we aim to determine the detailed parameters for the reported arc-melting process, which can provide useful insights on the synthesis of the Ti3SiC2 MAX phase by arc-melting process. Furthermore, we compared the electrical characteristics and densities of the three samples.

Keywords

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