Figure 1. Chemical structure of Red 167.
Figure 2. 5L class pilot scale supercritical CO2 dyeing machine.
Figure 3. Experimental equipment for supercritical fluid dyeing.
Figure 4. Dyeing cycle.
Figure 5. Colorimetric position.
Figure 6. Comparison of color difference and α along the PET mass.
Figure 7. Residual dye depending on PET mass.
Figure 8. Comparison of color difference and α along the dyeing time.
Figure 9. Color difference before and after cleaning along the dyeing time.
Figure 10. Capture of color difference before and after cleaning along the dyeing time.
Table 1. Information of fabric and dyestuff
References
- W. Saus, D. Knittel, and E. Schollmeyer, Dyeing of Textilesin Supercritical Carbon Dioxide, Tex. Res. J., 63(3), 135(1993). https://doi.org/10.1177/004051759306300302
- J. H. Kim, Theme : Supercritical Fluid, J. KSME, 55(7), 30(2015).
- E. Bach, E. Cleve, and E. P. Schollmeyer, Past, Present and Future of Supercritical Fluid Dyeing Technology, Rev. Prog. Color. Relat. Top., 32, 88(2002). https://doi.org/10.1111/j.1478-4408.2002.tb00253.x
- A. Hou, B. Chen, J. Dai, and K. Zhang, Using Supercritical Carbon Dioxide as Solvent to Replace Water in Polyetylene Terephthalate(PET) Fabric Dyeing Procedures, J. Clean Prod., 18, 1009(2010). https://doi.org/10.1016/j.jclepro.2010.03.001
- M. Banchero, S. Sicardi, A. Ferri, and L. Manna, Supercritical Dyeing of Textiles - From the Laboratory Apparatus to the Pilot Plant, Text. Res. J., 78, 217(2008). https://doi.org/10.1177/0040517507081297
- M. V. D. Kraan, Process and Equipment Development for Textile Dyeing in Supercritical Carbon Dioxide, Ph.D. Thesis, Delft University of Technology, 2005.
- J. J. Long, Y. Q. Ma, and J. P. Zhao, Investigations on the Level Dyeing of Fabrics in Supercritical Carbon Dioxide, J. Supercrit. Fluids, 57, 80(2011). https://doi.org/10.1016/j.supflu.2011.02.007
-
J. V. Schnitzler and R. Eggers, Mass Transfer in Polymers in a Supercritical
$CO_2$ -Atmosphere, J. Supercrit. Fluids, 16, 81(1999). https://doi.org/10.1016/S0896-8446(99)00020-0 - A. Hou, K. Xie, and J. Dai, Effect of Supercritical Carbon Dioxide Dyeing Conditions on the Chemical and Morphological Changes of Poly(ethylene terephthalate) Fibers, J. Appl. Polym. Sci., 92, 2008(2004). https://doi.org/10.1002/app.20066
- O. S. Fleming, S. G. Kazarian, E. Bach, and E. Schollmeyer, Confocal Raman Study of Poly(ethylene terephthalate) Fibres Dyed in Supercritical Carbon Dioxide: Dye Diffusion and Polymer Morphology, Polymer, 46, 2943(2005). https://doi.org/10.1016/j.polymer.2005.02.067
- M. V. D. Kraan, M. V. F. Cid, G. F. Woerlee, W. J. T. Veugelers, and G. J. Witkamp, Equilibrium Study on the Disperse Dyeing of Polyester Textile in Supercritical Carbon Dioxide, Text. Res. J., 77, 550(2007). https://doi.org/10.1177/0040517507077483
-
P. Bao and J. Dai, Relationships between the Solubility of C. I. Disperse Red 60 and Uptake on PET in Supercritical
$CO_2$ , J. Chem. Eng. Data, 50, 838(2005). https://doi.org/10.1021/je0496847 - M. W. Park and H. K. Bae, Dye Distribution in Supercritical Dyeing with Carbon Dioxide, J. Supercrit. Fluids, 22, 65(2002). https://doi.org/10.1016/S0896-8446(01)00102-4
- A. Ferri, M. Banchero, L. Manna, and S. Sicardi, Dye Uptake and Partition Ratio of Disperse Dyes between a PET Yarn and Supercritical Carbon Dioxide, J. Supercrit. Fluids, 37, 107(2006). https://doi.org/10.1016/j.supflu.2005.07.001
- H. D. Sung and J. J. Shim, Solubility of C.I. Disperse Red 60 and C.I. Disperse Blue 60 in Supercritical Carbon Dioxide, J. Chem. Eng. Data, 44, 985(1999). https://doi.org/10.1021/je990018t
- C. C. Tsai, H. Lin, and M. Lee, Solubility of Disperse Yellow 54 in Supercritical Carbon Dioxide with of without Cosolvent, Fluid Phase Equalibria, 260, 287(2007). https://doi.org/10.1016/j.fluid.2007.07.070
- K. H. Chang, H. K. Bae, and J. J. Shim, Dyeing of PET Textile Fibers and Films in Supercritical Carbon Dioxide, Korean J. Chem. Eng., 13(3), 310(1996). https://doi.org/10.1007/BF02705955
- I. I. Jung, S. Y. Lee, G. B. Lim, and J. H. Ryu, Supercritical Fluid Dyeing of Polyester Fiber with Two Different Dispersion Dyes, Clean Technology, 17(2), 110 (2011). https://doi.org/10.7464/KSCT.2011.17.2.110