TEM 정밀 시편 제작용 몰리브덴 합금 미세 고정 부품의 제작을 위한 절삭 가공 방법에 관한 연구

A study on machining method about molybdenum alloy micro fixing part for TEM precision specimen.

  • 김기범 (한국생산기술연구원 적층성형가공그룹) ;
  • 이창우 (한국생산기술연구원 적층성형가공그룹) ;
  • 이해진 (한국생산기술연구원 적층성형가공그룹) ;
  • 함민지 (한국생산기술연구원 적층성형가공그룹) ;
  • 김건희 (한국생산기술연구원 적층성형가공그룹)
  • Kim, Ki-Beom (Additive Manufacturing Process R&D Group, Korea Institute of Industrial Technology) ;
  • Lee, Chang-Woo (Additive Manufacturing Process R&D Group, Korea Institute of Industrial Technology) ;
  • Lee, Hae-Jin (Additive Manufacturing Process R&D Group, Korea Institute of Industrial Technology) ;
  • Ham, Min-Ji (Additive Manufacturing Process R&D Group, Korea Institute of Industrial Technology) ;
  • Kim, Gun-Hee (Additive Manufacturing Process R&D Group, Korea Institute of Industrial Technology)
  • 투고 : 2017.10.17
  • 심사 : 2017.11.24
  • 발행 : 2017.12.01

초록

In these days, increase requirement of TEM (Transmission Electro Microscope) in not only scientific field but also industrial field. Because TEM can measure inner-structure of specimen a variety of materials like metal, bio. etc. When use TEM, specimen should be thin about 50nm. So making for thin specimen, use Ion milling device that include specimen holder. The holder generally made of Aluminium Aluminium holder is worn away easily. For this reason, using time of ion milling with aluminum holder is too short. To solve the problem, we replace aluminium holer to molybdenum alloy holder. In this paper, we design molybdenum alloy holer for CAM and modify CAD modeling for effective machining process. So we array a specimen 3 by 4 and setup orientation for one-shot machining process. Next we make a CAM program for machining. we making a decision two machining strategy that chose condition of tool-path method, step-down, step-over. etc. And then conduct machining using CNC milling machining center. To make clear difference between case.1 and case.2, we fixed machining conditions like feed-rate, main spindle rpm, etc. After machining, we confirm the condition of workpiece and analysis the problems case by case. Finally, case.2 work piece that superior than case.1 cutting with WEDM because that method can not ant mechanical effect on workpiece.

키워드

참고문헌

  1. A. Loynuk, D. Poppitz, U. R. J. W. Gerlach, F. Frost, S. Bemutz, E. Thelander, B. Rauschenbach, "Focused high- and low-energy ion milling for TEM specimen preparation", Microelectronics Reliability, Vol. 55, Issues 9-10, pp. 2119-2125, 20115. https://doi.org/10.1016/j.microrel.2015.07.005
  2. J. Li, T. Mails, S. Dionne, "Recent abvances in FIB-TEM specimen preparation techniques", Materials Characterization, Vol. 57, Issue 1, pp. 64-70, 2006. https://doi.org/10.1016/j.matchar.2005.12.007
  3. Yu. B. Kuz'ma, "An X-Ray structural investigation of the systems niobium-titanium-boron and niobium-molybdenum-boron" Soviet Power Metallurgy and Metal Ceramics Vol. 10 Issue 4, pp. 298-300, 1971.
  4. R. Steinitz, I. Binder, D. Moskowitz, "System Molybdenum-Boron and Some Properties of The Molybdenum-Borides", JOM, Vol 4, Issue 9, pp. 983-987, 1952. https://doi.org/10.1007/BF03397758
  5. F. Morito, N. I. Danylenko, H. Saito, A. V. Krajnikov, "Boron Distribution and Micrestructure in Molybhenum-Boron Alloys" Metallic Materials with High Structural Efficiency, Vol 146, pp. 347-354, 2004.
  6. C. A. Spindt, I. Brodie, L. Humphrey, and E. R. Westerberg, "Physical properties of thin film field emission cathodes with molybdenum cones" Journal of Applied Physics, Vol 47, Issue 12, pp. 5248, 1976. https://doi.org/10.1063/1.322600
  7. 최규완, 장성호, "사각뿔/원뿔 형상의 마이크로니들 가공 기술 개발", 한국금형공학회지 제10권 제3호, 25-29, 2016.
  8. 문영대, "DMLS와 NC복합가공기의 실용성 검토", 한국금형공학회지 제9권 제3호, 34-40, 2016.
  9. 배성환, 민경호, "기계적 특성 향상을 위한 마그네슘 합금의 등틍로각압출 공정 조건에 관한 연구", 한국금형공학회지 제10권 제1호, 12-18, 2016.