DOI QR코드

DOI QR Code

Evaluation of Microstructure and Mechanical Property of Inconel 600 Degraded under High Temperature

고온 열화된 Inconel 600강의 미세조직 및 기계적 특성 평가

  • Jung, Kwang-Hu (Division of Marine Engineering, Mokpo National Maritime University) ;
  • Kim, Seong-Jong (Division of Marine Engineering, Mokpo National Maritime University)
  • 정광후 (목포해양대학교 기관시스템공학부) ;
  • 김성종 (목포해양대학교 기관시스템공학부)
  • Received : 2017.12.11
  • Accepted : 2017.12.21
  • Published : 2017.12.31

Abstract

In this study, we investigated the effect of thermal aging on mechanical characteristics of Inconel 600 nickel-based alloy. The thermal aging was conducted up to 1000 hours at an atmosphere of $650^{\circ}C$. The microstructure of thermally aged specimens was investigated by an optical microscope (OM), scanning electron microscope (SEM) and energy dispersive spectrometer (EDS). In addition, tensile test (strain rate: 2 mm/min) and micro Vickers hardness test were conducted to evaluate mechanical properties with time. As a result of the experiment, Cr-rich carbide continuously precipitated during thermal aging, leading to the change of the mechanical characteristics and fracture mode. With the increase of aging time, tensile strength, yield strength, and hardness gradually decreased. The fracture mode changed from ductile to brittle with the increase of grain boundary carbide.

Keywords

References

  1. P. Viklund, Superheater corrosion in biomass and waste fired boilers: characterisation, causes and prevention of chlorine-induced corrosion, (2013) (Doctoral dissertation, KTH Royal Institute of Technology).
  2. D. B. Lee, High-temperature Corrosion by Chlorides in Biomass-fired Plants, J. Kor. Inst. Surf. Eng., 49 (2016) 14-19. https://doi.org/10.5695/JKISE.2016.49.1.14
  3. G. Bai, J. Li, R. Hu, Z. Tang, X. Xue, H. Fu, Effect of temperature on tensile behavior of Ni- Cr-W based superalloy, Mater. Sci. Eng. A., 528 (2011) 1974-1978. https://doi.org/10.1016/j.msea.2010.11.053
  4. F. Mechehoud, N. E. Benaioun, N. E. Hakiki, A. Khelil, L. Simon, J. L. Bubendorff, Thermally oxidized Inconel 600 and 690 nickel-based alloys characterizations by combination of global photoelectrochemistry and local near-field microscopy techniques (STM, STS, AFM, SKPFM), Appl. Surf. Sci., 433 (2018) 66-75. https://doi.org/10.1016/j.apsusc.2017.10.094
  5. H. Y. Zhang, Y. H. Lu, M. Ma, J. Li, Effect of precipitated carbides on the fretting wear behavior of Inconel 600 alloy, Wear., 315 (2014) 58-67. https://doi.org/10.1016/j.wear.2014.03.012
  6. H. Sahlaoui, H. Sidhom, J. Philibert, Prediction of chromium depleted-zone evolution during aging of Ni-Cr-Fe alloys, Acta Mater., 50 (2002) 1383- 1392. https://doi.org/10.1016/S1359-6454(01)00444-X
  7. C. Stawstrom, M. Hillert, Improved depleted-zone theory of intergranular corrosion of 18-8 stainless steel, J. Iron. Steel. Inst., 207 (1969) 77-85.
  8. J. D. Wang, D. Gan, Effects of grain boundary carbides on the mechanical properties of Inconel 600, Mater. Chem. Phys., 70 (2001) 124-128. https://doi.org/10.1016/S0254-0584(00)00484-3
  9. Y. Guo, B. Wang, S. Hou, Aging precipitation behavior and mechanical properties of inconel 617 superalloy, Acta Metall. Sin., 26 (2013) 307-312. https://doi.org/10.1007/s40195-012-0249-3
  10. X. Bai, J. Pan, G. Chen, J. Liu, J. Wang, T. Zhang, and W. Tang, Effect of high temperature aging on microstructure and mechanical properties of HR3C heat resistant steel, Mater. Sci. and Tech., 30 (2014) 205-210. https://doi.org/10.1179/1743284713Y.0000000347
  11. A. Iseda, H. Okada, H. A. Semba and M. Igarashi, Long term creep properties and microstructure of SUPER304H, TP347HFG and HR3C for A-USC boilers, Energy Mater., 2 (2007) 199-206. https://doi.org/10.1179/174892408X382860
  12. J. J. Kai, C. H. Tsai, T. A. Huang, M. N. Liu, The effects of heat treatment on the sensitization and SCC behavior of INCONEL 600 alloy, Metall. Trans. A., 20 (1989) 1077-1088. https://doi.org/10.1007/BF02650143
  13. A. Gunen, E. Kanca, Microstructure and Mechanical Properties of Borided Inconel 625 Superalloy, Materia (Rio Janeiro)., 22 (2017).
  14. R. C. Scarberry, S. C. Pearman, J. R. Crum, Precipitation reactions in Inconel Alloy 600 and their effect on corrosion behavior. Corros. Sci., 32 (1976) 401-406. https://doi.org/10.5006/0010-9312-32.10.401
  15. W. Y. Maeng, T. W. Nam, The Effects of Heat Treatment on Intergranular Carbide Precipitations and Intergranular Stress Corrosion Cracking of Inconel alloy, J. Korean Soc. Heat Treat., 10 (1997) 219-231.
  16. E. L. Hall, C. L. Briant, The microstructural response of mill-annealed and solution-annealed INCONEL 600 to heat treatment, Metall. Mater. Trans. A., 48, 16 (1985) 1225-1236.
  17. Y. F. Yin, R. G. Faulkner, Model predictions of grain boundary chromium depletion in Inconel 690, Corros. Sci., 49 (2007) 2177-2197. https://doi.org/10.1016/j.corsci.2006.10.022
  18. J. M. Larson, Carbide morphology in p/m IN-792. Metall. Trans. A., 7 (1976) 1497-1502. https://doi.org/10.1007/BF02656391