Journal of the Korean Magnetic Resonance Society (한국자기공명학회논문지)

Korean Magnetic Resonance Society (한국자기공명학회)
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The Role of NMR in the Field of Quantitative Analysis

  • Received : 2016.08.10
  • Accepted : 2016.09.05
  • Published : 2016.09.20
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Abstract

Although NMR technique has been using in many areas of chemistry, its merit on quantitative analysis seems not to acknowledge greatly because of the many inferior intrinsic aspects, particularly its sensitivity. Recently, new NMR techniques, high-field NMR, and demands for cutting edge techniques of analysis, however, seem to change the role of NMR spectroscopy in this field. This review shows the application of NMR development in quantitative analysis and will discuss the basic idea, limitations, and pitfalls. Then it will show you several successful applications applied in quantitative analysis and you will see how useful and accurate method it is.

Keywords

References

  1. E. D. Becker, High resolution NMR, Academic Press, New York. (1980)
  2. F. A. L. Anet, and D. J. O'Leary, Tetrahedron Lett. 30, 1059 (1989) https://doi.org/10.1016/S0040-4039(01)80358-0
  3. D. L. Rabenstein, K. K. Millis, and E. J. Strauss, Anal. Chem. 60, 1380 (1988) https://doi.org/10.1021/ac00165a006
  4. D. L. Rabenstein, and D. A. Keire, Pract. Spectrosc. 11, 323 (1991)
  5. L. D. Field, and S. Sternhell, Analytical NMR, John Wiley & Sons, Chichester. (1989)
  6. Sigma-Aldrich, Analytic, 4, 14 (2007)
  7. Sigma-Aldrich, Analytic, 2, 9 (2010)
  8. V. Silvestre, S. Goupry, M. Trierweiler, R. Robins, and S. Akoka, Anal. Chem. 73, 1862 (2001) https://doi.org/10.1021/ac0013204
  9. M. Thunhorst, and U. Holzgrabe, Magn. Reson. Chem. 36, 211 (1998) https://doi.org/10.1002/(SICI)1097-458X(199803)36:3<211::AID-OMR246>3.0.CO;2-Y
  10. T. H. Ahn, H. C. Kang, and S.G. Lee, Bull. Korean Chem. Soc. 13, 577 (1992)
  11. S. G. Lee, Personal communication
  12. H. S. Lim, G. G. Han, and S. G. Lee, Bull. Korean Chem. Soc. 23, 1507 (2002) https://doi.org/10.5012/bkcs.2002.23.11.1507
  13. H. S. Lim, and S. G. Lee, Bull. Korean Chem. Soc. 27, 972 (2006) https://doi.org/10.5012/bkcs.2006.27.7.972
  14. S. G. Lee, J. Kor. Magn. Reson. Soc. 11, 115 (2007)
  15. S. G. Lee, Bull. Korean Chem. Soc. 28, 1635 (2007) https://doi.org/10.5012/bkcs.2007.28.10.1635
  16. H. S. Lim, C. J. Park, and S. G. Lee, Anal. Sci. Technol. 21, 438 (2008)
  17. G. B. Park, C. J. Park, and S. G. Lee, Anal. Sci. Technol. 20, 400 (2007)