Korean Journal of Veterinary Service (한국동물위생학회지)

The Korean Society of Veterinary Service (한국동물위생학회)
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Monitoring for cephalosporins residues in raw meat in Seoul

서울지역 유통 식육 중의 세팔로스포린계 항균물질 잔류실태 조사

  • Kim, Mi-Ran (Seoul Metropolitan Government Research Institute of Public Health ＆ Environment) ;
  • Choi, Yoon-Hwa (Seoul Metropolitan Government Research Institute of Public Health ＆ Environment) ;
  • Choi, Hoon (Seoul Metropolitan Government Research Institute of Public Health ＆ Environment) ;
  • Kim, Doo-Hwan (Seoul Metropolitan Government Research Institute of Public Health ＆ Environment) ;
  • Kim, Young-Seob (Seoul Metropolitan Government Research Institute of Public Health ＆ Environment) ;
  • Lee, Ju-Hyung (Seoul Metropolitan Government Research Institute of Public Health ＆ Environment)
  • 김미란 (서울특별시보건환경연구원) ;
  • 최윤화 (서울특별시보건환경연구원) ;
  • 최훈 (서울특별시보건환경연구원) ;
  • 김두환 (서울특별시보건환경연구원) ;
  • 김영섭 (서울특별시보건환경연구원) ;
  • 이주형 (서울특별시보건환경연구원)
  • Received : 2015.08.07
  • Accepted : 2015.12.16
  • Published : 2015.12.30
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Abstract

We investigated the residues of 6 cephalosporins (cefquinome, cephalexin, cephalonium, cefazolin, ceftiofur, cefuroxime) using LC-MS/MS in raw meat in Seoul. This method involves extraction of the residue from the meat by distilled water and methanol followed by a manual of residue analysis published by the National Institute of Food and Drug Safety Evaluation. The recoveries ranged between 74.71~90.01% in beef, 73.37~101.40% in pork and 70.87~95.53% in chicken, respectively. The limits of detection were 0.0004~0.0563 mg/kg, and the limits of quantification were 0.001~0.169 mg/kg respectively. Residues of cephalosporins which exceeded maximum residue limits (MRL) were not exceed in any of the 287 samples. However, it is necessary to develop multi-method, which includes the active metabolites of ceftiofur.

Keywords

References

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