Bulletin of the Korean Chemical Society

Korean Chemical Society (대한화학회)
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A Manganese Coordination Polymer and a Palladium Molecular Compound of 3-Pyridinepropionic acid (HL): [MnL2(H2O)2]∞ and trans-[Pd(HL)2Cl2]

  • Im, Seo Young (Department of Chemistry, Sungkyunkwan University, Natural Science Campus) ;
  • Lee, Soon W. (Department of Chemistry, Sungkyunkwan University, Natural Science Campus)
  • Received : 2013.06.19
  • Accepted : 2013.07.11
  • Published : 2013.10.20
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Abstract

Three coordination polymers, [$ML_2(H_2O)_2$] (M = Co (1), Ni (2), Mn (3)), were prepared from metal acetates ($M(CH_3COO)_2{\cdot}4H_2O$) and 3-pyridinepropionic acid ($HL=(3-py)-CH_2CH_2COOH$) by solvent-layer methods. By contrast, a discrete molecular compound, trans-[$Pd(HL)_2Cl_2$] (4), was synthesized by replacing benzonitrile (PhCN) ligands in trans-[$Pd(PhCN)_2Cl_2$] with HL under microwave-heating conditions. Compounds 1-3 have a 2D framework, and compound 4 contains a square-planar Pd metal.

Keywords

References

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