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http://dx.doi.org/10.5012/bkcs.2013.34.10.2947

A Manganese Coordination Polymer and a Palladium Molecular Compound of 3-Pyridinepropionic acid (HL): [MnL2(H2O)2]∞ and trans-[Pd(HL)2Cl2]  

Im, Seo Young (Department of Chemistry, Sungkyunkwan University, Natural Science Campus)
Lee, Soon W. (Department of Chemistry, Sungkyunkwan University, Natural Science Campus)
Publication Information
Bulletin of the Korean Chemical Society / v.34, no.10, 2013 , pp. 2947-2952 More about this Journal
Abstract
Three coordination polymers, [$ML_2(H_2O)_2$] (M = Co (1), Ni (2), Mn (3)), were prepared from metal acetates ($M(CH_3COO)_2{\cdot}4H_2O$) and 3-pyridinepropionic acid ($HL=(3-py)-CH_2CH_2COOH$) by solvent-layer methods. By contrast, a discrete molecular compound, trans-[$Pd(HL)_2Cl_2$] (4), was synthesized by replacing benzonitrile (PhCN) ligands in trans-[$Pd(PhCN)_2Cl_2$] with HL under microwave-heating conditions. Compounds 1-3 have a 2D framework, and compound 4 contains a square-planar Pd metal.
Keywords
Pyridyl-carboxylate terminals; Coordination polymer;
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