Analysis of Wide-gap Semiconductors with Superconducting XAFS Apparatus

  • Shiki, S. (Advanced Industrial Science and Technology (AIST)) ;
  • Zen, N. (Advanced Industrial Science and Technology (AIST)) ;
  • Matsubayashi, N. (Advanced Industrial Science and Technology (AIST)) ;
  • Koike, M. (Advanced Industrial Science and Technology (AIST)) ;
  • Ukibe, M. (Advanced Industrial Science and Technology (AIST)) ;
  • Kitajima, Y. (High Energy Accelerator Research Organization (KEK)) ;
  • Nagamachi, S. (Ion Technology Center Co. Ltd.) ;
  • Ohkubo, M. (Advanced Industrial Science and Technology (AIST))
  • Received : 2012.12.17
  • Accepted : 2012.12.24
  • Published : 2012.12.31

Abstract

Fluorescent yield X-ray absorption fine structure (XAFS) spectroscopy is useful for analyzing local structure of specific elements in matrices. We developed an XAFS apparatus with a 100-pixel superconducting tunnel junction (STJ) detector array with a high sensitivity and a high resolution for light-element dopants in wide-gap semiconductors. An STJ detector has a pixel size of $100{\mu}m$ square, and an asymmetric layer structure of Nb(300 nm)-Al(70 nm)/AlOx/Al(70 nm)-Nb(50 nm). The 100-pixel STJ array has an effective area of $1mm^2$. The XAFS apparatus with the STJ array detector was installed in BL-11A of High Energy Accelerator Research Organization, Photon Factory (KEK PF). Fluorescent X-ray spectrum for boron nitride showed that the average energy resolution of the 100-pixels is 12 eV in full width half maximum for the N-K line, and The C-K and N-K lines are separated without peak tail overlap. We analyzed the N dopant atoms implanted into 4H-SiC substrates at a dose of 300 ppm in a 200 nm-thick surface layer. From a comparison between measured X-ray Absorption Near Edge Structure (XANES) spectra and ab initio FEFF calculations, it has been revealed that the N atoms substitute for the C site of the SiC lattice.

Keywords

References

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