Effect of Electron Beam Currents on Stabilization of Polyacrlonitrile Precursor Fiber

PAN 전구체 섬유의 안정화시 전자선 전류의 영향

  • Shin, Hye Kyoung (Radiation Research Division for Industry & Environment, Advanced Radiation Technology Institute, Korea Atomic Energy Research Institute) ;
  • Jeun, Joon Pyo (Radiation Research Division for Industry & Environment, Advanced Radiation Technology Institute, Korea Atomic Energy Research Institute) ;
  • Kim, Hyun bin (Radiation Research Division for Industry & Environment, Advanced Radiation Technology Institute, Korea Atomic Energy Research Institute) ;
  • Kang, Phil Hyun (Radiation Research Division for Industry & Environment, Advanced Radiation Technology Institute, Korea Atomic Energy Research Institute)
  • 신혜경 (한국원자력연구원 정읍방사선과학연구소 공업환경연구부) ;
  • 전준표 (한국원자력연구원 정읍방사선과학연구소 공업환경연구부) ;
  • 김현빈 (한국원자력연구원 정읍방사선과학연구소 공업환경연구부) ;
  • 강필현 (한국원자력연구원 정읍방사선과학연구소 공업환경연구부)
  • Received : 2011.02.18
  • Accepted : 2011.03.06
  • Published : 2011.03.30

Abstract

Polyacrylonitrile (PAN) fibers are the most widely used precursor of the materials for carbon fibers. The conventional process of carbon fibers from PAN precursor fiber includes two step; stabilization at low temperature and carbonization at high temperature. Compared to thermal stabilization, the stabilization process by electron beam (E-beam) irradiation is a advanced and brief method. However, a stabilization by E-beam irradiation was required a high dose (over 5,000 kGy) and spend over 1.5 hr (1.14 MeV, 1 mA). In the present work the main goal is exploring a quick stabilization process by cotrolling E-beam currents. The effect of various E-beam currents on stabilization of PAN precursor fiber was studied by gel fraction test, thermo gravimertic analysis (TGA), differential scanning calorimetry (DSC), tensile strength, and scanning electron microscopy (SEM) images.

Keywords

Acknowledgement

Supported by : 교육과학기술부