한국분말재료학회지 (Journal of Powder Materials)

  • 제17권5호
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  • Pages.409-414
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  • 2010
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  • 2799-8525(pISSN)
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  • 2799-8681(eISSN)
한국분말재료학회 (*구 분말야금학회) (The Korean Powder Metallurgy & Materials Institute)
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Characterization of TiO2 Synthesized in Acidic Conditions at Low Temperature by Sol-gel Method

  • 투고 : 2010.08.30
  • 심사 : 2010.10.08
  • 발행 : 2010.10.28
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초록

Titanium dioxide ($TiO_2$), which is one of the most basic materials in our daily life, plays a key role for environment purification. We synthesized $TiO_2$ nanoparticles by the hydrolysis reactions of titanium tetraisopropoxide using $HNO_3$ as a peptizing agent or $CH_3COOH$ as a chelating agent in the sol-gel method. The powder consisted of a rod shape or a spherical shape according to the concentration and kind of acid. The physical properties of $TiO_2$ nanoparticles were investigated with X-ray diffraction, SEM, BET analysis, and UV-Vis spectrophotometer.

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참고문헌

  1. M. Kaneko and I. Okura: Photocatalysis Science and Technology, Kodansha Ltd., Tokyo,. Springer-Verlag Berlin Heidelberg, New York (2002) 1.
  2. I. A. Montoya, T. Vireros, J. M. Dominguez, L. A. Canales and I. Schifter: Catal. Lett., 15 (1992) 207. https://doi.org/10.1007/BF00770913
  3. M. E. Simonsen and E. G. Søgaard: J. Sol-Gel Sci. Technol., 53 (2010) 458.
  4. W. Y. Wu, Y. M. Chang and J. M. Ting: Cryst. Growth Des., 10 (2010) 1646. https://doi.org/10.1021/cg901210c
  5. Y. Wang, L. Zhang, K. Deng, X. Chen and Z. Zou: J. Phys. Chem. C, 111 (2007) 2709. https://doi.org/10.1021/jp066519k
  6. A. C. Lee, R. H. Lin, C. Y. Yang, M. H. Lin and W. Y. Wang: Mater. Chem. Phys., 109 (2008) 275. https://doi.org/10.1016/j.matchemphys.2007.11.016
  7. R. Benedix, F. Dehn, J. Quaas and M. Orgass: Lacer, 5 (2000) 157.
  8. K. Thamaphat, P. Limsuwan and B. Ngotawornchai: Kasetsart J. Nat. Sci., 42 (2008) 357.
  9. C. Ribeiro, C. Vila, D. B. Stroppa, V. R. Mastelaro and J. Bettini: J. Phys. Chem. C, 111 (2007) 5871. https://doi.org/10.1021/jp070051j
  10. T. D. Nguyen-Phan, V. H. Pham, T. V. Cuong, S. H. Hahn, E. J. Kim, J. S. Chung, S. H. Hur and E. W. Shin: Mater. Lett., 64 (2010) 1387. https://doi.org/10.1016/j.matlet.2010.03.033
  11. K. S. W. Sing, D. H. Everett, R. A. W. Haul, L. Moscou, R. A. Pierotti, J. Rouquerol and T. Siemieniewska: Pure & Appl. Chem., 57 (1985) 603. https://doi.org/10.1351/pac198557040603
  12. S. Lowell and J. E. Shields: Powder Surface Area and Porosity, Third Edition, Chapman and Hall, New York (1991) 11.