DOI QR코드

DOI QR Code

Synthesis of Gold Nanoparticles by Chemical Reduction Method for Direct Ink Writing

  • Cho, Young-Sang (Nano Functional Materials Research Group, Department of Powder Materials, Korea Institute of Materials Science) ;
  • Son, Soo-Jung (Nano Functional Materials Research Group, Department of Powder Materials, Korea Institute of Materials Science) ;
  • Kim, Young-Kuk (Nano Functional Materials Research Group, Department of Powder Materials, Korea Institute of Materials Science) ;
  • Chung, Kook-Chae (Nano Functional Materials Research Group, Department of Powder Materials, Korea Institute of Materials Science) ;
  • Choi, Chul-Jin (Nano Functional Materials Research Group, Department of Powder Materials, Korea Institute of Materials Science)
  • 투고 : 2010.07.28
  • 심사 : 2010.09.27
  • 발행 : 2010.10.28

초록

Aqueous gold nanoparticle dispersion was synthesized by chemical reduction method using diethanolamine as reducing agent and polyethyleneimine as dispersion stabilizer. The synthesis conditions for the stable dispersion of the gold nanoparticle suspension were determined by changing the amount of the reducing agent and dispersant during the wet chemical synthesis procedures. The face centered cubic lattice structure of the gold nanoparticles was confirmed by using X-ray diffraction and the morphologies of the nanoparticles were observed by transmission electron microscope. The synthesized gold nanoparticle dispersion was concentrated by evaporating the dispersion medium at room temperature followed by the addition of ethyleneglycol as humectant for the increase of the elastic properties to obtain gold nanoparticle inks for direct ink writing process. The line patterns were obtained with the gold nanoparticle inks during the writing procedures and the morphologies of the fine patterns were observed by scanning electron microscope.

키워드

참고문헌

  1. M. Oda and J. Surf: Finishing Soc. Jpn., 47 (1996) 910. https://doi.org/10.4139/sfj.47.910
  2. http://www.utilisegold.com/assets/file/utilisegold/pdf/JM.pdf
  3. J. B. Szczech, C. M. Megaridis, J. Zhang, and D. R. Gamota: Nanosc. Microsc. Thermophys. Eng., 8 (2004) 327. https://doi.org/10.1080/10893950490516884
  4. J. J. Sotrhoff, R. Elghanian, R. C. Mucic, C. A. Mirkin and R. L. Letsinger: J. Am. Chem. Soc., 120 (1998) 1959. https://doi.org/10.1021/ja972332i
  5. Y. Sun, A. I. Frenkel, H. White, L. Zhang, Y. Zhu, H. Xu, J. C. Yang, T. Koga, V. Zaitsev, M. H. Rafailovich and J. C. Sokolov: J. Phys. Chem. B, 110 (2006) 23022. https://doi.org/10.1021/jp060432h
  6. P.-Y. Silvert, K. and Tekaia-Elhsissen: Solid State Ionics, 82 (1995) 53. https://doi.org/10.1016/0167-2738(95)00198-F
  7. T. Li, H. G. Park and S.-H. Choi: Mater. Chem. Phys., 105 (2007) 325. https://doi.org/10.1016/j.matchemphys.2007.04.069
  8. A. Iwakoshi, T. Nanke and T. Kobayashi: Gold Bull., 38 (2005) 107. https://doi.org/10.1007/BF03215244
  9. T. Sakura, T. Takahashi, K. Kataoka and Y. Nagasaki: Colloid Polym. Sci., 284 (2005) 97. https://doi.org/10.1007/s00396-005-1339-9
  10. S. K. Rhodes, R. H. Lambeth, J. Gonzales, J. S. Moore, and J. A. Lewis: Langmuir, 25 (2009) 6787. https://doi.org/10.1021/la9003092
  11. W. B. Russel, D. A. Saville and W. R. Showalter: Colloidal Dispersion, Cambridge University Press, New York (1999).
  12. B. Y. Ahn, E. B. Duoss, M. J. Motala, X. Guo, S.-I. Park, Y. Xiong, J. Yoon, R. G. Nuzzo, J. A. Rogers, and J. A. Lewis: Sci., 323 (2009) 1590.
  13. S. Link and M. A. El-Sayed: J. Phys. Chem. B, 103 (1999) 4212. https://doi.org/10.1021/jp984796o
  14. B. Y. Ahn, D. Shoji, C. J. Hansen, E. Hong, D. C. Dunand and J. A. Lewis: Adv. Mater., 22 (2010) 1. https://doi.org/10.1002/adma.201090021

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