Bulletin of the Korean Chemical Society

Korean Chemical Society (대한화학회)
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A Comparison Method of Silver Nanoparticles Prepared by the Gamma Irradiation and in situ Reduction Methods

  • Lee, Chul-Jae (Division of Chemical Industry, Yeungnam College of Science & Technology) ;
  • Karim, Mohammad Rezaul (Center of Excellence for Research in Engineering Materials, College of Engineering, King Saud University) ;
  • Vasudevan, T. (Department of Chemistry Education, Kyungpook National University) ;
  • Kim, Hee-Jin (Department of Chemistry Education, Kyungpook National University) ;
  • Raushan, K. (Department of Chemistry Education, Kyungpook National University) ;
  • Jung, Maeng-Joon (School of Nano & Materials Science Engineering, Kyungpook National University) ;
  • Kim, Dong-Yeub (Division of Chemical Industry, Yeungnam College of Science & Technology) ;
  • Lee, Mu-Sang (Department of Chemistry Education, Kyungpook National University)
  • Received : 2010.03.25
  • Accepted : 2010.05.25
  • Published : 2010.07.20
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Abstract

Silver nanoparticles has been prepared by the $\gamma$-irradiation and in situ reduction methods. Based on the Raman spectra, TEM images, X-ray Diffraction (XRD) patterns and UV-vis spectra, the in situ reduction method is more stable and the average size of the silver nanoparticles is also smaller than by the $\gamma$-irradiation reduction method. It is identified that the silver ions interacting with nonbonding electrons of oxygen atom in the carbonyl group of polyvinylpyrrolidone (PVP) by the in situ reduction method. It is also found advantages of the in situ reduction method including no additional reducing agents, without $\gamma$-irradiations treatment and the room temperature treatment suitability.

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